Abstract:Schematic of a GCE fabricated with SnO2·ZnO·TiO2 NMs/Nafion/GCE using a conducting Nafion binder and its electrochemical response as a benzaldehyde sensor.
“…The end application of an electrochemical sensor should be the detection of real samples collected from various environmental sources. [50][51][52][60][61][62] Therefore, the assembled sensor based on Ag$NiMn 2 O 4 nanomaterial/binder/GCE was applied to analyze a number of samples obtained from various environmental sources, such as a PC baby bottle, PC water bottle, industrial waste effluent, and PVC food packaging bag; the resulting data obtained by applying the recovery method are summarized in Table 4. As illustrated in Table 4, the data were deemed to be quite acceptable.…”
Section: Analysis Of Real Samples By the Recovery Methodsmentioning
confidence: 99%
“…The calcinations converted the carbonates of the sample into their oxides. 51,52 Three different single metal oxides (Ag 2 O, NiO and MnO) were also synthesized by the same method. All these oxides were calcined at 950 C. The reactions of the Ag$NiMn 2 O 4 synthesis can be summarized as below: For size analysis, a Williamson-Hall plot (eqn (1)) was used; the particle size was estimated to be 58.3 nm, where the standard deviation (ESD) of the peak tting is 0.00039 ( Fig.…”
Section: Synthesis Of the Ag$nimn 2 O 4 Nanocompositementioning
confidence: 99%
“…Finally, the study indicated that trimetallic oxide nanocomposites are promising candidates for photocatalytic applications and environmental protection due to their nanostructure formation and perturbations of electronic energy levels. 51,52,[60][61][62] Anti-bacterial activity of the Ag$NiMn 2 O 4 nanocomposite…”
Section: Kinetics Study Of Methyl Violet 6b Degradation By the Ag$nimmentioning
Photocatalytic dye degradation efficiency of Ag·NiMn2O4 at pH 4 was 91%; at pH 9, 77% and 95% in presence of H2O2 and at pH 7, 50%. Assembled Ag·NiMn2O4 nanomaterials/binder/GCE, as m-THyd sensor showed considerable sensitivity, DL, LDR, response time, reproducibility etc.
“…The end application of an electrochemical sensor should be the detection of real samples collected from various environmental sources. [50][51][52][60][61][62] Therefore, the assembled sensor based on Ag$NiMn 2 O 4 nanomaterial/binder/GCE was applied to analyze a number of samples obtained from various environmental sources, such as a PC baby bottle, PC water bottle, industrial waste effluent, and PVC food packaging bag; the resulting data obtained by applying the recovery method are summarized in Table 4. As illustrated in Table 4, the data were deemed to be quite acceptable.…”
Section: Analysis Of Real Samples By the Recovery Methodsmentioning
confidence: 99%
“…The calcinations converted the carbonates of the sample into their oxides. 51,52 Three different single metal oxides (Ag 2 O, NiO and MnO) were also synthesized by the same method. All these oxides were calcined at 950 C. The reactions of the Ag$NiMn 2 O 4 synthesis can be summarized as below: For size analysis, a Williamson-Hall plot (eqn (1)) was used; the particle size was estimated to be 58.3 nm, where the standard deviation (ESD) of the peak tting is 0.00039 ( Fig.…”
Section: Synthesis Of the Ag$nimn 2 O 4 Nanocompositementioning
confidence: 99%
“…Finally, the study indicated that trimetallic oxide nanocomposites are promising candidates for photocatalytic applications and environmental protection due to their nanostructure formation and perturbations of electronic energy levels. 51,52,[60][61][62] Anti-bacterial activity of the Ag$NiMn 2 O 4 nanocomposite…”
Section: Kinetics Study Of Methyl Violet 6b Degradation By the Ag$nimmentioning
Photocatalytic dye degradation efficiency of Ag·NiMn2O4 at pH 4 was 91%; at pH 9, 77% and 95% in presence of H2O2 and at pH 7, 50%. Assembled Ag·NiMn2O4 nanomaterials/binder/GCE, as m-THyd sensor showed considerable sensitivity, DL, LDR, response time, reproducibility etc.
“…However, the electrochemical techniques are advantageous in terms of sensitivity, low-cost, response-time, and pretreatment of samples not required so suitable for on-field detection [ 22 , 23 , 24 , 25 , 26 ]. Thus electrochemical techniques gain substantial consideration in recent years [ 27 , 28 , 29 , 30 , 31 , 32 ]. Still, interference from similar chemicals is often observed in spectrophotometric techniques.…”
Herein, a novel copper-doped gadolinium oxide (Cu-doped Gd2O3; CGO) nanofiber was synthesized by a simple solution method in the basic phase and successfully characterized. We have used Fourier Transform Infrared Spectroscopy (FTIR), X-ray Diffraction (XRD), Field Emission Scanning Electron Microscope (FESEM) and Energy-Dispersive Spectroscopy (EDS) techniques for characterization of the CGO nanofiber. The CGO nanofiber was used later to modify Au-coated μ-Chips with poly(3,4-ethylenedioxythiophene) polystyrene sulfonate (PEDOT:PSS) polymer mixtures (coating binder) to selectively detect 4-cyanophenol (4-CP) in an aqueous medium. Notable sensing performance was achieved with excellent sensitivity (2.4214 µAµM−1 cm−2), fast response time (~12 s), wide linear dynamic range (LDR = 1.0 nM–1.0 mM: R2 = 0.9992), ultra-low detection limit (LoD; 1.3 ± 0.1 pM at S/N = 3), limit of quantification (LoQ; 4.33 pM), and excellent reproducibility and repeatability for CGO/Au/μ-Chip sensor. This CGO modified Au/μ-chip was further applied with appropriate quantification and determination results in real environmental sample analyses.
“…This study was conducted to synthesize and characterize a tri-metal oxide from single metal oxides of interest, for exploring electrochemical sensor applications, because trimetallic oxide nanocomposites are promising systems for toxin sensors, photocatalytic applications and environmental safety, an efficient anti-bacterial agent against MDR bacteria, and industrial sterilization mediators. [12][13][14][15][16] Phenolic compounds and their derivatives are extensively used in the production of pharmaceuticals, dyes, pesticides, etc., and are known as severe environmental toxins. 17,18 They cause severe damage to organisms and plants.…”
A tri-metal oxides, MoO2∙Fe3O4∙CuO (TMO) was synthesized by the co-precipitation method and characterized by XRD, SEM-EDS, and FTIR. The average particle size of the nanocomposite was found to be 34.85...
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