Articles you may be interested inMicrostructural and crystallographic imperfections of MgB2 superconducting wire and their correlation with the critical current density AIP Advances 4, 017113 (2014) In a sequel to our previous paper (J. Appl. Phys. 113, 036908 (2013)), where we reported comprehensive analysis of inter-grain connectivity (A F ), pinning, percolation threshold (P c ), and anisotropy (c) in a series of ex-situ processed MgB 2 , we address the same issues in in-situ processed samples. MgB 2 samples with stoichiometric composition, excess Mg (5 wt. %) and further 3 wt. % addition of various non-carbon based additives like nano-Ag, nano-Ni, and YBCO are synthesised by the in-situ route. Detailed investigations of X-ray diffraction, magnetization (M), and resistivity (q) as a function of temperature (T) and field (B) in the range 5-300 K and 0-8 T are carried out in all the samples. The resistive superconducting onset T con $ 38.6 6 0.3 K and offset (where q goes to zero) T c0 $ 38.1 6 0.3 K of the samples stay nearly unchanged. The inter-grain connectivity (A F ) of the samples varies between 11%-20%. All the additives result in a critical current density (J c ) higher than the stoichiometric MgB 2 sample, where the highest values (e.g., J c (1 T, 5 K) $ 1.2 Â 10 9 A/m 2 ) are observed for the sample with 5 wt. % excess Mg. The major findings based on quantitative analysis of q (T, B) and J c (B, T) data in all the samples are: (1) along with previously studied ex-situ samples, the J c (A F ) shows a significant increase at A F $ 7%; (2) the irreversibility lines lie lower than the characteristic T c0 (B) lines in the B-T phase diagram; (3) a universal core pinning (dl-and/or dT c -type) mechanism is revealed in the entire T range 5-30 K; and (4) typical values of P c $ 0.57 6 0.04 is indicative of weak link networks. V C 2014 AIP Publishing LLC.