Abstract:Small titania particles, prepared by hydrolysis and condensation using in situ steric stabilization, have been studied by high-energy, transmission, electron energy-loss spectroscopy. Electron diffraction patterns and energy-loss spectra as a function of momentum transfer were measured for as-prepared particles (amorphous titania), particles annealed at 600 ± C (primarily anatase), and particles annealed at 1000 ± C (primarily rutile). The energy-loss spectra at low momentum disagreed with the loss function ca… Show more
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