“…and solvents were water + 0,05% trifluoroacetic acid (TFA, purity >99%, Laboratoire MAT, Québec, QC, Canada) for phase A and acetonitrile (HPLC grade, EMD Chemicals Inc., Gibbstown, NJ, USA) + 0.05% TFA for phase B. All other parameters of the HPLC method were the same as those used by Labbé, Araya-Farias, Tremblay, and Bazinet (2005) which were based on the National Institute of Standards and Technology method (Dalluge, Nelson, Thomas, & Sander, 1998).…”