Electrodeposition of poly(3,4-ethylenedioxythiophene) on a stainless steel wire for solid phase microextraction and GC determination of some esters with high boiling points
“…2c). Compared with previously reported cauliflower-like PEDOT coating [11], the PEDOT-IL/GNs was more porous and wrinkled, with larger available surface area, which benefited extraction. The formation of folded and wrinkled structure was due to the doping of IL/GNs.…”
Section: Morphological Structure and Compositions Of Pedot-il/gns Coamentioning
confidence: 58%
“…Poly(3,4-ethylenedioxythiophene) (PEDOT) and its derivatives are among the most frequently investigated conductive polymers due to their high mechanical strength, excellent chemical and thermal stability and electrical conductivity [7][8][9]. These properties also make PEDOT favorable adsorbent for SPME of some organic compounds such as organochlorine pesticides [10] and esters [11].…”
“…2c). Compared with previously reported cauliflower-like PEDOT coating [11], the PEDOT-IL/GNs was more porous and wrinkled, with larger available surface area, which benefited extraction. The formation of folded and wrinkled structure was due to the doping of IL/GNs.…”
Section: Morphological Structure and Compositions Of Pedot-il/gns Coamentioning
confidence: 58%
“…Poly(3,4-ethylenedioxythiophene) (PEDOT) and its derivatives are among the most frequently investigated conductive polymers due to their high mechanical strength, excellent chemical and thermal stability and electrical conductivity [7][8][9]. These properties also make PEDOT favorable adsorbent for SPME of some organic compounds such as organochlorine pesticides [10] and esters [11].…”
“…6), both composite layers exhibit a cauliower-like structure, which is typical for poly (3,4-ethylenedioxythiophene). 65,[75][76][77] In the case of (p)N-CNTs/pEDOT/PSS composite the presence of (p)N-CNTs is clearly visible in the SEM images. Plasma treated carbon nanotubes create entangled networks that increase porosity of the nanocomposite.…”
Section: Characterization Of Nanocomposite (P)n-cnts/pedot/ Pssmentioning
In this work we present a simple and efficient method of nitrogen plasma modification of carbon nanotubes (CNTs). The process allows for treatment of the nanotubes in the form of powder with quite a high yield (65 mg of CNTs per hour). The modified carbon nanotubes contain approx. 3.8% nitrogen, mostly in the pyridinic form. Plasma treated CNTs exhibit better dispersibility in water and higher electric capacitance than pristine CNTs. Modified CNTs are a proper component of novel nanocomposites based on the conducting polymer poly(3,4-ethyleneidoxythiophene). Electrodeposited thin layers of the nanocomposite exhibit improved electrochemical properties (higher capacitance, better stability, lower resistance, faster diffusion) compared to the pure polymer layers.
“…From the PVA/PEDOT nanofiber spectrum, peaks of PVA nanofibers can still be seen, proving the presence of PVA nanofibers after electrodeposition of PEDOT. Three characteristic peaks of PEDOT are observed at 775, 1318 and 1602 cm −1 , indicating the C=S, C-C [29], C-C [30] stretching band of thiophene ring in PEDOT structure, respectively. In addition, the C-C stretching of the thiophene ring of PEDOT was observed at 1602 cm −1 [30].…”
Poly(vinyl alcohol)/poly(3,4-ethylenedioxythiophene) (PVA/PEDOT) nanofibers were synthesized as a positive electrode for high-performance asymmetric supercapacitor (ASC). PVA/PEDOT nanofibers were prepared through electrospinning and electrodeposition meanwhile reduced graphene oxide (rGO) was obtained by electrochemical reduction. The PVA/PEDOT nanofibers demonstrated cauliflower-like morphology showing that PEDOT was uniformly coated on the smooth cross-linking structure of PVA nanofibers. In addition, the ASC showed a remarkable energy output efficiency by delivering specific energy of 21.45 Wh·kg−1 at a specific power of 335.50 W·kg−1 with good cyclability performance (83% capacitance retained) after 5000 CV cycles. The outstanding supercapacitive performance is contributed from the synergistic effects of both PVA/PEDOT//rGO, which gives promising materials for designing high-performance supercapacitor applications.
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