The work described was carried out with the hope of finding a definite answer, either positive or negative, to the question, "Can zirconium be electrodeposited from solution?" Attempts were made to electrodeposit zirconium and, in some cases, zirconium alloys from numerous aqueous and nonaqueous solutions. None of the solutions used gave a weighable electrodeposit of pure zirconium but some solutions gave thin cathode deposits which contained zirconium and iron. No work with fused salt baths for zirconium is included.