2014
DOI: 10.1016/j.electacta.2014.08.055
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Electrochemical growth of porous titanium dioxide in a glycerol-based electrolyte at different temperatures

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Cited by 41 publications
(20 citation statements)
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References 63 publications
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“…This linear dependence, suggesting that the reaction kinetics is limited by the mass transfer in the electrolyte, is different from the exponential trends observed for anodization of other metals, e.g. Al[12,[38][39][40], or Ti[13,41, 42]. This could be explained by the semiconducting nature of oxide, its relatively high porosity and, what is more important, the fact, that the resulting current is related with both the formation of the oxide layer as well as with the vigorous oxygen evolution at the anode.…”
contrasting
confidence: 65%
See 1 more Smart Citation
“…This linear dependence, suggesting that the reaction kinetics is limited by the mass transfer in the electrolyte, is different from the exponential trends observed for anodization of other metals, e.g. Al[12,[38][39][40], or Ti[13,41, 42]. This could be explained by the semiconducting nature of oxide, its relatively high porosity and, what is more important, the fact, that the resulting current is related with both the formation of the oxide layer as well as with the vigorous oxygen evolution at the anode.…”
contrasting
confidence: 65%
“…In the case when aluminum or titanium was anodized, both pore diameter (D p ) and cell size (pore to pore distance -D c ) are strongly affected by anodizing conditions, especially anodizing potential. A lot of publications report strong linear relationships between D p and D c and applied potential [12,13,[37][38][39][40][41][42].…”
Section: Figurementioning
confidence: 99%
“…After the first and second steps, the ATO layers were mechanically removed from Ti surface and the samples were immediately reanodized. 14,23,24 After the third oxidation step, the samples were rinsed with water, air-dried, and sterilized by ethylene oxide. The structure and morphology of fabricated ATO samples were verified by a field emission scanning electron microscope (FE-SEM; Hitachi S-4700).…”
Section: Experimental Scaffold Preparationmentioning
confidence: 99%
“…It is also a low cost and simple method [1,12]. Kapusta-Kołodziej et al [13] reported that the effectiveness of TiO 2 NT depends evidently on TiO 2 layers. The layers of TiO 2 NT can be controlled by several parameters such as electrolyte concentration, pH, temperature, anodizing voltage, anodizing time and calcination temperature [14].…”
Section: Introductionmentioning
confidence: 99%