Effects of pH in photoreduction by hydrazine

Inbar, Shai; Cohen, Saul G.

doi:10.1021/ja00482a029

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1978

2001

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Cited by 12 publications

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“…spectrum of 2,4-methano-3,3-d2-2,4-dehydroadamantane (1a).12 (12) Compound 1a was prepared by pyrolysis of the tosylhydrazone sodium salt of 4-methylene-d2-2-adamantanone. (13) Stothers, J.…”

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confidence: 99%

Primary quantum yields of ketyl radicals in photoreduction by amines. Abstraction of hydrogen from nitrogen

Inbar¹,

Linschitz²,

Cohen³

1980

J. Am. Chem. Soc.

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Communications to the Editor 1419 product sublimed into a trap cooled by liquid nitrogen and was found to be more than 95% pure by 13C NMR.The structure proof for 1 is based on the mass spectrum1 la (m/e 146 (M+)), the IR spectrum1 la (v 3040 cm-1), the NMR spectrum ((CeDe) 2.36-1.06 (multiplet and two distinctive doublets at 2.12 and 1.08, J = 4 Hz1 lb)), and the 13C NMR spectrum ((C6D6) b 64.4 (d,

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confidence: 99%