Effective Role of Two Layers of Silica in the Performance of Fe3O4@xSiO2@ySiO2@BisPyP-Ni Core-Shell Catalyst for C-C and C-S Coupling Reactions

Saleh, Ebraheem Abdu Musad; Kassem, Asmaa F.; Altalbawy, Farag M. A.; Shoja, Sarah Jawad; Bokov, Dmitry Olegovich; Elawady, Ahmed; Al-Rubaye, Ameer H.; Saud, Abdulnaser; Al-Mashhadani, Zuhair I.; Nejad, Maryam Sadat Ghorayshi

doi:10.1007/s12633-024-02959-0

Silicon

2024

DOI: 10.1007/s12633-024-02959-0

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Effective Role of Two Layers of Silica in the Performance of Fe3O4@xSiO2@ySiO2@BisPyP-Ni Core-Shell Catalyst for C-C and C-S Coupling Reactions

Ebraheem Abdu Musad Saleh,

Asmaa F. Kassem,

Farag M. A. Altalbawy

et al.

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Green Synthesis of Quinazolinones via Selective Electro‐oxidation Using Iron Electrode and NaCl Electrolyte as an Eco‐friendly Electrolyte

Basem,

Naglah,

Alaridhee

et al. 2024

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Primary alcohols 2(a–h) and o‐aminobenzamides 1(a–h) can be selectively oxidized electrochemically to yield dihydroquinazolinone 4(a–h) and quinazolinones 5(a–h) in an efficient and chemoselective manner. This methodology employs sodium chloride (NaCl) 3(a) as a co‐catalyst and electricity as the oxidizing agent, utilizing cost‐effective and commercially available materials such as Graphite anode, Iron (Fe) cathode, and isopropyl alcohol (iPrOH) as a solvent and weak base. The synthesis yields various quinazolinone derivatives with diverse structural characteristics in good quantities, showcasing the method‘s broad applicability. This approach facilitates the production of a range of dihydroquinazolinones and quinazolinones (24 examples), highlighting its versatility and compatibility with different functional groups. Characterization of the synthesized derivatives included CHN analysis, 1HNMR spectroscopy, and determination of melting points.

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Green Synthesis of Quinazolinones via Selective Electro‐oxidation Using Iron Electrode and NaCl Electrolyte as an Eco‐friendly Electrolyte

Basem,

Naglah,

Alaridhee

et al. 2024

ChemistrySelect

View full text Add to dashboard Cite

show abstract

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Effective Role of Two Layers of Silica in the Performance of Fe3O4@xSiO2@ySiO2@BisPyP-Ni Core-Shell Catalyst for C-C and C-S Coupling Reactions

Cited by 1 publication

References 63 publications

Green Synthesis of Quinazolinones via Selective Electro‐oxidation Using Iron Electrode and NaCl Electrolyte as an Eco‐friendly Electrolyte

Green Synthesis of Quinazolinones via Selective Electro‐oxidation Using Iron Electrode and NaCl Electrolyte as an Eco‐friendly Electrolyte

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