Effect of the type and level of hydration of alcoholic solvents on the simultaneous extraction of oil and chlorogenic acids from sunflower seed press cake

Scharlack, Nayara K; Aracava, Keila Kazue; Rodrigues, Christianne Elisabete da Costa

doi:10.1002/jsfa.8331

Cited by 22 publications

(18 citation statements)

References 45 publications

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“…Alcoholic solvents presented accumulated extraction yields higher than 90%, however, IPA0 presents better performance (96.3 ± 0.1%) when compared to Et0 (92 ± 1%) ( p < 0.05). Previous studies comparing the performance of Et0 and IPA0 have shown that with the latter is achieved higher oil extraction yields, which may be related to the lower polarity of IPA0.…”

Section: Resultsmentioning

confidence: 92%

Macadamia Oil Extraction With Alcoholic Solvents: Yield and Composition of Macadamia Oil and Production of Protein Concentrates From Defatted Meal

Navarro

Rodrigues

2018

Euro J Lipid Sci & Tech

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The aim of this study is to evaluate the performance of ethanol and isopropanol in the extraction of macadamia oil and the production of protein concentrates from the defatted meal. Partially defatted macadamia cake is submitted to batch extractions in one stage of contact at 60, 75, and 90 °C, while the sequential extraction trials considering four stages are performed at 75 °C. Oil extraction yield is influenced by the solvent type, temperature, and pre‐treatment of the material. Absolute isopropanol at 90 °C enables to extract 66% of the oil while in the sequential configuration, oil yield up to 96% is attained after four stages. The retention of the solution adhered to the fiber (liquid holdup, LH) is affected by the type of solvent and characteristics of the raw material, being obtained LH values higher than 2. The oil extraction conditions affect negatively on the nitrogen solubility index of the defatted meal. The solvents in absolute degree impact less on the solubility of the proteins, enabling the production of macadamia protein concentrates (protein content of 70%) with functional properties suitable for using in the food industry. Practical Applications: This study is useful to oilseed processors and researchers because it addresses the issue of using macadamia cake as raw material to oil extraction with alcoholic solvents, ethanol, and isopropanol, which are less flammable and toxic than hexane. In addition, it is evaluated the effect of process variables on the oil yield, liquid holdup, and characteristics of the extraction products (oil and defatted meal). The results of this work could help to develop macadamia oil extraction process safe for the workers of oil industry and consumers and, simultaneously, to enable the use of by‐products (defatted meal) in the protein concentrates production. Macadamia oil extraction, from partially defatted macadamia cake, is carried out using ethanol and isopropanol (absolute and hydrated) as solvents. The products of macadamia oil extraction are characterized, thus the extracted oils show typical fatty acid composition and the defatted meal presented higher protein content than raw material. Therefore, from these defatted meals are produced macadamia protein concentrates, which show good functional properties to be used as food ingredients.

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Section: Resultsmentioning

confidence: 92%

Macadamia Oil Extraction With Alcoholic Solvents: Yield and Composition of Macadamia Oil and Production of Protein Concentrates From Defatted Meal

Navarro

Rodrigues

2018

Euro J Lipid Sci & Tech

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“…The same did not happen in mass yield and, or deacidification yield, because, as shown in Figures 3 and 4, the results of yield do not comply the number of contacts. This demonstrates that the solvent has more affinity with fatty acids, and the losses in the process refer to the neutral oil drag (Sawada, Venâncio, Toda, & Rodrigues, 2014; Scharlack et al, 2017; Toda, Sawada, & Rodrigues, 2016).…”

Section: Resultsmentioning

confidence: 98%

“…Some works suggest to replace it with green solvents such as ethanol and isopropanol, or such as mechanical extraction without solvent (Araújo et al, 2018; Bessa, Ferreira, Rodrigues, Batista, & Meirelles, 2017; Cornelio‐Santiago, Mazalli, Rodrigues, & Oliveira, 2019). Furthermore, modern methods such as aqueous, enzymatic extraction with microwaves, ultrasound, or supercritical fluids can be used (Gaber, Tujillo, Mansour, & Juliano, 2018; Koubaa, Mhemdi, & Vorobiev, 2016; Scharlack, Aracava, & Rodrigues, 2017), increasing the extraction yield and maintaining oil quality (Sánchez, Fernández, & Nolasco, 2017).…”

Section: Introductionmentioning

confidence: 99%

Improving quality of refined canola oil byliquid–liquidextraction on pilot scale apparatus

Tiritan

Tonial

Dalmolin

et al. 2020

J Food Process Engineering

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The aim of this work was to refine expeller‐pressed crude canola oil by pilot scale liquid–liquid extraction with hydrated ethanol as solvent. Quality indices were determined, and shelf life was estimated in the accelerated test. The scale projection was performed based on the results of the pilot scale. The experimental device operates in a batch process with 89.6% yield deacidification and an average of 4.4 contacts per assay. In this process, without bleaching and deodorization steps, physicochemical parameters were according to the Codex Alimentarius standards, except moisture. In this way, it will be necessary to apply nonthermal techniques to remove water. The major fatty acids identified were oleic and linoleic acid and the absence of trans fatty acids. For the shelf life, the refined oil presented free fatty acids 0.28% and peroxide value 12.65 meq O2 kg−1 after 24 hr at 65°C. The pilot scale results showed that the technique is suitable to produce edible oils. A liquid–liquid extractor was designed for industrial scale with the total volume will be 12,000 L. To process 6 tons of crude canola oil per day, the unit will be able to produce 1.3 thousand tons per year of refined canola oil. Practical applications After acid degumming, canola oil was submitted to liquid–liquid extraction, using ethanol as solvent. As a result, two traditional steps of refining vegetable oils have been eliminated: bleaching and deodorization. This fact directly impacts on physical space of industry, maintenance of equipment and need for operators. Trans fats were not detected in canola oil, pointing that the technique is efficient in the production of healthier oils, with less environmental impact.

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“…Estudos relatam a utilização de etanol na extração de óleo de algodão (MAGNE e SKAU, 1953;RAO e ARNOLD, 1958;HRON e KOLTUN, 1984;ABRAHAM et al, 1991ABRAHAM et al, , 1993HRON et al, 1994); amendoim (KAPARTHI e CHARI, 1959;FONSECA e REGITANO-d'ARCE, 1993), avelã (FRANCO et al, 2009buriti (RIBEIRO et al, 2010); café e girassol (FREITAS e LAGO, 2007);castanha-do-Brasil (FREITAS et al, 2007); girassol (REGITANO-d'ARCE, 1985, 1991REGITANO-d'ARCE et al, 1994;SINEIRO et al, 1998;SCHARLACK et al, 2017); milho (KWIATKOWSKI e CHERYAN, 2002;CHIEN et al, 2002;; pinhão-manso (BROSSARD-GONZALEZ et al, 2010); rosa rubiginosa (FRANCO et al, 2007); sementes de uva (FERNANDEZ et al, 2010); farelo de arroz (RODRIGUES e OLIVEIRA, 2010;OLIVEIRA et al, 2012a;KAMIMURA et al, 2017;BESSA et al, 2017;) e soja (BECKEL et al, 1946, 1948bARNOLD e CHOUDHURY, 1962;LAGO et al, 1985;SILVA e TURATTI, 1991;RITTNER, 1992;GANDHI et al, 2003;SAWADA et al, 2014;TODA et al, 2016). No caso do solvente isopropanol são encontrados na literatura trabalhos utilizando-se algodão (HARRIS et al, 1947(HARRIS et al, , 1949HARRIS e HAYWARD, 1950;...…”

Section: Emprego De Solventes Alternativos Na Extração De óLeo De Matunclassified

“…No LES também foram conduzidos estudos que objetivaram delimitar as condições de extração em termos de temperatura e hidratação do solvente alcoólico para a extração de óleo de soja laminada e estudo que avaliou o impacto das condições de processo sobre o número de estágios do extrator sólido-líquido e sobre a etapa de recuperação do solvente por resfriamento da miscela oriunda do processo de extração (OLIVEIRA et al, 2012b). A influência das variáveis do processo de extração, tipo de solvente alcoólico e temperatura, sobre as características físico-químicas do óleo de soja (SAWADA et al, 2014), óleo de gérmen de milho , óleo de sementes de girassol (SCHARLACK et al, 2017) e óleo de farelo de arroz foi também estudada pelo Grupo de Pesquisa do LES.…”

Section: Introductionunclassified

Viabilidade técnica do emprego de solventes alcoólicos na extração de óleos vegetais: caracterização físico-química do óleo, funcionalidades da fração proteica e recuperação do solvente

Capellini¹

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O correr da vida embrulha tudo. A vida é assim: esquenta e esfria, aperta e daí afrouxa, sossega e depois desinquieta. O que ela quer da gente é coragem." João Guimarães Rosa Dedico este trabalho aos meus pais e minha irmã, Ary, Maria e Maria Eduarda, e ao meu melhor amigo e companheiro, Bruno. À eles todo o meu amor e eterna gratidão! AGRADECIMENTOS Agradeço, em primeiro lugar, a Deus pela vida, pela minha família e amigos, pela proteção diária e pela força para superar qualquer tipo de obstáculo. Agradeço aos meus pais, Ary e Maria, minha irmã, Maria Eduarda, minhas avós, Tereza e Marina, meus avôs, Antônio (in memorian) e Benedito (in memorian), tios, tias, primo e primas, por todo amor e apoio incondicionais. Agradeço ao Bruno por sempre ser o meu porto seguro, pelo apoio e companheirismo em todas as situações e pela paciência em lidar com meus muitos momentos de ansiedade durante esses anos de Doutorado. Agradeço à minha orientadora Christianne Elisabete da Costa Rodrigues pela confiança depositada em mim e em meu trabalho, pela paciência, pela oportunidade de aprendizado, pelo carinho e amizade nestes 8 anos de parceria. Chris, o seu amor, cuidado e dedicação me contagiam mesmo nos momentos mais difíceis, fazendo com que toda essa caminhada valha a pena. Agradeço à Keila pelas palavras de carinho, pelo cuidado comigo, pela amizade e parceria em todos os momentos. Agradeço aos amigos Daniel, Cristina e Diane pelo apoio nos momentos mais difíceis de toda esta jornada, pelas risadas, pela companhia (mesmo que de longe), pelos conselhos e por todo amor que recebo de vocês. Agradeço aos amigos de Americana, Piracicaba, Pirassununga, aos que estão em tantos outros lugares mas que contribuíram de maneira fundamental com amor, alegria, apoio nos momentos difíceis, paciência...sem a contribuição de cada um de vocês este caminho teria sido muito mais árduo. A todos os amigos do Laboratório de Engenharia de Separações pelo carinho, parceria e ensinamentos diários. Aos alunos de Iniciação Científica, que passaram ou ainda permanecem no Laboratório de Engenharia de Separações, Vanessa, Larissa, Cristiane, Helder, Bruno, Ingrid, Camila e Juliana pela ajuda no desenvolvimento deste trabalho. Aos técnicos, especialistas e professores responsáveis

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Effect of the type and level of hydration of alcoholic solvents on the simultaneous extraction of oil and chlorogenic acids from sunflower seed press cake

Cited by 22 publications

References 45 publications

Macadamia Oil Extraction With Alcoholic Solvents: Yield and Composition of Macadamia Oil and Production of Protein Concentrates From Defatted Meal

Macadamia Oil Extraction With Alcoholic Solvents: Yield and Composition of Macadamia Oil and Production of Protein Concentrates From Defatted Meal

Improving quality of refined canola oil byliquid–liquidextraction on pilot scale apparatus

Viabilidade técnica do emprego de solventes alcoólicos na extração de óleos vegetais: caracterização físico-química do óleo, funcionalidades da fração proteica e recuperação do solvente

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