Effect of the Silicon Drift Detector on EDAX Standardless Quant Methods

Eggert, Frank

doi:10.1017/s1551929519001196

Cited by 12 publications

(4 citation statements)

References 20 publications

Supporting

Mentioning

Contrasting

Order By: Relevance

“…The MThin models were set up to account for absorption and material density using the default Zaluzec option, and then run assuming constant sample thicknesses of 0.5 μm, 0.75 μm, and 1 μm to establish general trends. More information about these models can be found in references [17] and [18], respectively.…”

Section: Methodsmentioning

confidence: 99%

Quantitative SEM-EDS Analysis of Semi-Transparent Samples

Boona

2021

Micros. Today

View full text Add to dashboard Cite

show abstract

Section: Methodsmentioning

confidence: 99%

Quantitative SEM-EDS Analysis of Semi-Transparent Samples

Boona

2021

Micros. Today

View full text Add to dashboard Cite

show abstract

“…The acquisition time for each EDS spectrum was no <10 minutes. The EDS characteristic spectra were analyzed by the standardless eZAF method 30 for semiquantitative compositional analysis. The atomic number correction factor (Z), absorption correction factor (A), secondary fluorescence correction factor (F), and total error (Err %) are provided in Table S1.…”

Section: Methodsmentioning

confidence: 99%

Mechanochemically assisted synthesis of titanium carbonitride from metal and organic precursor

Liu

et al. 2020

J Am Ceram Soc

View full text Add to dashboard Cite

Ultrafine TiC0.29N0.38 powders with a particle size of approximately 170 nm were synthesized by mechanochemical synthesis combined with moderate‐temperature annealing using Ti and ethylenediamine as raw materials. Ethylenediamine plays a versatile role in the fabrication of ultrafine TiCxNy powders. It can serve as not only carbon and nitrogen sources, but also a process control agent, that facilitates the generation of ultrafine particles. A dense TiC0.3N0.39 ceramic with a high hardness of 16.7 GPa was obtained by spark plasma sintering at a considerably reduced temperature of 1100°C. This simple, energy‐efficient method is a novel approach to synthesizing valuable TiCxNy.

show abstract

“…Measurements were acquired by either an EDAX Apollo XV detector or an EDAX Octane Elect EDS System mounted on a Zeiss Ultra55 field-emission scanning electron microscope (SEM) operated at 6.5 kV. The EDX quantification process was performed using the standardless eZAF algorithm provided by EDAX [17]. The composition analysis of (In, Ga)As nanowires was complemented by the utilization of scanning transmission electron microscopy (STEM) with high-resolution energy-dispersive x-ray spectroscopy (EDX).…”

Section: Characterizationmentioning

confidence: 99%

Composition and optical properties of (In, Ga)As nanowires grown by group-III-assisted molecular beam epitaxy

Ruiz,

Castro,

Herranz

et al. 2024

Nanotechnology

View full text Add to dashboard Cite

(In,Ga) alloy droplets are used to catalyse the growth of (In,Ga)As nanowires by molecular beam epitaxy on Si(111) substrates. The composition, morphology and optical properties of these nanowires can be tuned by the employed elemental fluxes. To incorporate more than 10% of In, a high In/(In+Ga) flux ratio above 0.7 is required. We report a maximum In content of almost 30% in bulk (In,Ga)As nanowires for an In/(In+Ga) flux ratio of 0.8. However, with increasing In/(In+Ga) flux ratio, the nanowire length and diameter are notably reduced. Using photoluminescence and cathodoluminescence spectroscopy on nanowires covered by a passivating (In,Al)As shell, two luminescence bands are observed. A significant segment of the nanowires shows homogeneous emission, with a wavelength corresponding to the In content in this segment, while the consumption of the catalyst droplet leads to a spectrally-shifted emission band at the top of the nanowires. The (In,Ga)As nanowires studied in this work provide a new approach for the integration of infrared emitters on Si platforms.

show abstract

Effect of the Silicon Drift Detector on EDAX Standardless Quant Methods

Abstract: Abstract

Cited by 12 publications

References 20 publications

Quantitative SEM-EDS Analysis of Semi-Transparent Samples

Quantitative SEM-EDS Analysis of Semi-Transparent Samples

Mechanochemically assisted synthesis of titanium carbonitride from metal and organic precursor

Composition and optical properties of (In, Ga)As nanowires grown by group-III-assisted molecular beam epitaxy

Contact Info

Product

Resources

About