Abstract:Chickpea starch was modified by heat-moisture treatment (HMT). The effect of heat-moisture treatment on the amylose content of chickpea starch was studied, and the physicochemical properties, gelatinization properties, texture properties and digestion properties of modified chickpea starch were compared and analyzed by scanning electron microscopy (SEM), X-ray diffraction (XRD) and Fourier transform infrared (FT-IR). After HMT, the amylose content of chickpea starch increased. Compared with the natural starch,… Show more
“…The peaks in the C1 region are typical characteristics of V-type single helices (eight glucose cycles per round), while those around C4 are amorphous crossing points associated with the amylopectin double helix (Liu et al, 2019;Sudlapa & Suwannaporn, 2023; DEWI et al Xie et al, 2020). HMT decreases the percentage of double helices and increases single helices, resulting in a higher moisture content treatment and reduced relative crystallinity (Du et al, 2023;Wang et al, 2018).…”
Section: Identification and Prediction Of Hmt-osa Starch Molecular St...mentioning
This study presented the impact of pH and octenyl succinic anhydride (OSA) concentration on the esterification reaction of heat-moisture-treated sago starch (HMT-S) using response surface methodology to achieve optimum degree of substitution (DS), reaction efficiency (RE), and water contact angle (CA). The results showed that HMT-OSA sago starch (HMT-OS) starch exhibited an optimum pH of 7.26 and an OSA concentration of 4.53%. The DS value, RE, and water CA of optimized HMT-OS starch were 0.0121, 33.07%, and 90.11°, respectively. Furthermore, the optimized HMT-OS was used to evaluate the effect of starch modification on film characteristics. HMT-OS film has the best moisture-proof and mechanical properties compared to control (NS), HMT-S, and N-OS films, as indicated by lower water vapor permeability (28.69 g H2O.mm/s.m2.Pa × 10-11), water solubility (26.61%), higher CA (104.40°), elongation at break (85.63%), and transparency (3.25% mm-1). According to the scanning electron micrographic images, the absence of cracks or pores was attributed to the waterproof properties and flexibility of the film. Conversely, x-ray diffraction results showed that the crystallinity of HMT-OS film decreased to 36.05%.
“…The peaks in the C1 region are typical characteristics of V-type single helices (eight glucose cycles per round), while those around C4 are amorphous crossing points associated with the amylopectin double helix (Liu et al, 2019;Sudlapa & Suwannaporn, 2023; DEWI et al Xie et al, 2020). HMT decreases the percentage of double helices and increases single helices, resulting in a higher moisture content treatment and reduced relative crystallinity (Du et al, 2023;Wang et al, 2018).…”
Section: Identification and Prediction Of Hmt-osa Starch Molecular St...mentioning
This study presented the impact of pH and octenyl succinic anhydride (OSA) concentration on the esterification reaction of heat-moisture-treated sago starch (HMT-S) using response surface methodology to achieve optimum degree of substitution (DS), reaction efficiency (RE), and water contact angle (CA). The results showed that HMT-OSA sago starch (HMT-OS) starch exhibited an optimum pH of 7.26 and an OSA concentration of 4.53%. The DS value, RE, and water CA of optimized HMT-OS starch were 0.0121, 33.07%, and 90.11°, respectively. Furthermore, the optimized HMT-OS was used to evaluate the effect of starch modification on film characteristics. HMT-OS film has the best moisture-proof and mechanical properties compared to control (NS), HMT-S, and N-OS films, as indicated by lower water vapor permeability (28.69 g H2O.mm/s.m2.Pa × 10-11), water solubility (26.61%), higher CA (104.40°), elongation at break (85.63%), and transparency (3.25% mm-1). According to the scanning electron micrographic images, the absence of cracks or pores was attributed to the waterproof properties and flexibility of the film. Conversely, x-ray diffraction results showed that the crystallinity of HMT-OS film decreased to 36.05%.
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