The microstructural and textural evolution and changes in Grain Boundary Character Distribution (GBCD) during annealing of a prior cold worked (30 %, 50 % and 80 %) Fe-C martensitic steel have been studied, and correlated with mechanical properties. It has been demonstrated that ultrafine grains in the range 50-250 nm can be obtained by choosing appropriate amounts of cold rolling and annealing. Increasing the annealing temperature in all the three materials produces the expected results, namely decrement of strength with a concomitant increase in ductility. Although reasonably sharp g-fibres were obtained in most of the cases, the very low r-bar values (Ͻ1.0) make the steels unsuitable for deep drawing purposes. It has been suggested that grain boundary engineering may lead to better strength-ductility combinations in this steel for enhanced range of applications.KEY WORDS: texture; cold rolling; annealing; mechanical properties; Grain Boundary Character Distribution; martensite. rolling mill with a roll diameter of 250 mm. The rolling was performed at a roll peripheral speed of 27.5 m · min Ϫ1 with machine oil as lubricant. The cold rolling could be successfully done without any edge cracking. Specimens of 15 mm in width and 100 mm in length were cut from the cold rolled sheets along the rolling direction (RD) for subsequent annealing and mechanical testing. The annealing of the cold rolled specimens was carried out at different temperatures ranging from 200-700°C, for 30 min with an interval of 100°C. From the annealed samples tensile specimens were prepared in accordance with ASTM E8M-04 standard and were subsequently polished. Tensile tests of polished samples were carried out at room temperature in Instron 4 210 machine with a constant cross-head speed of 0.5 mm · min
Ϫ1. The bulk hardness values (H v ) were calculated from the average of seven separate measurements taken at randomly selected points by using a load of 5 kg for 15 s. A detailed microstructural characterization was performed using Field Emission Gun Scanning Electron Microscope (FEG-SEM) and Transmission Electron Microscope (TEM). Specimens after etching with 2 % Nital, were observed along the cross section in a FEG-SEM operated at 15 kV. Thin foil TEM study was conducted in a PHILIPS CM200 TEM operated at 100 kV. Thin foils were prepared by twin jet electro polishing using a solution of 10 % HClO 4 ϩ90 % CH 3 COOH. Global texture measurements were carried out on the half thicknesses of the 30 %, 50 % and 80 % cold rolled as well as annealed (at 500°C and 700°C) samples using X-ray Diffraction (XRD) method in a PANalytical MRD machine. The (110), (200), (112) and (222) pole figures were determined, from which the Orientation Distribution Functions (ODFs) were calculated using the method of Bunge.
11)The grain boundary characterization was carried out in FEG-SEM operated at 20 kV equipped with an OIM/EBSD attachment. Samples after polishing with colloidal silica, were put in the sample holder of the SEM/EBSD equipment. Using a step size of 1....