Heat treatment of silanized feldspathic ceramic: effect on the bond strength to resin after thermocycling, International Journal of Adhesion and Adhesives, http://dx.Heat treatment of silanized feldspathic ceramic: effect on the bond strength to resin after thermocycling AbstractPurpose: This study aimed to evaluate the effect of heat treatment (at 77°C) of a silanized feldspathic ceramic on microtensile bond strength (μTBS) with a resin cement before and after being aged by thermocycling. Material and methods: Twenty-four blocks (12×10×4 mm) of a CADCAM feldspathic ceramic (Vitablocks Mark II, Vita) were obtained and randomly divided into three groups, according to the surface treatment prior to the cementation: Group AS -hydrofluoric acid 10% + silane; Group S77 -Silane + heating at 77°C for 60 s; and Group AS77 -hydrofluoric acid 10% + silane + heating at 77°C for 60 s.Ceramic blocks were cemented to composite resin blocks with a resin cement. The sets were subsequently cross-sectioned into 1 mm 2 beams for μTBS testing. The beams of each group were randomly divided into two subgroups: aging (thermocycling, 12,000 cycles between 5ºC and 55ºC) and non-aging (tested immediately). One-way ANOVA and Tukey's test (α = 0.05) and Weibull analysis (95% CI) were used to analyze the data. Results: Group AS77 had the lowest pre-test failure number during the cutting among the groups. There was no significant difference (p = 0.255) between the μTBS mean values of the non-aged groups. After aging, the mean value of S77 was significantly lower than those of AS77 and AS (p = 0.005).There was no difference in the Weibull modulus (m) and characteristic strength (σ o ) of the aged and nonaged groups for all comparisons. Before aging, heat treatment of silanized feldspathic ceramic (nonacid=etched surface) demonstrated bond strength similar to that achieved with hydrofluoric-acidetching treatment; however, it had lower bond strength after aging. Conclusion: The combination of hydrofluoric-acid-etching treatment with heat treatment silanized feldspathic ceramic did not improve the bond strength of the interface.