DSC investigation of chain cooperativity rearrangements and critical length scale of polybutadiene networks in glass transition range

Grigoraş, Vasile Cristian

doi:10.1007/s10973-022-11400-w

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Phase Sequence Seen Using the Dsc Methods1

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2023

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“…Therefore, the continuous step in heat flow from the glassy state to the supercooled state is observed in the thermogram. 21 Fig. 5 presents the DSC curves measured upon cooling the melted sample of AZP.…”

Section: Resultsmentioning

confidence: 99%

“…Therefore, the continuous step in heat flow from the glassy state to the supercooled state is observed in the thermogram. 21 one continuous step in heat flow at a temperature of 296.1 K and an exothermal anomaly around 350 K are observed at a low cooling rate of 2 K min −1 . Table 1 shows the phase transition temperatures depending on the rate of temperature change.…”

Section: Phase Sequence Seen Using the Dsc Methodsmentioning

confidence: 97%

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