Freeze-dried meat has been shown to be a desirable product with respect to versatility and acceptability (18).Another necessary requiremelit for a dehydrated food is good storage stability at relatively high temperatures. The deterioration of freeze-dried beef can be quite extensive under adverse conditions or extended storage. The mechanism of oxidative deterioration has been the subject of previous research (17). Since the oxidative deterioration of the freeze-dried meat must be eliminated by packing under vacuum or inert gas, in practice the non-oxidative deteriorative reactions become the most important factor in storage.I n his review 011 dehydrated meat Sharp (14) bas indicated that oxidation can be extensive. However, it becomes insignificant when the dehydrated meat is compressed or packed under nitrogen. Under these conditions the non-oxidative reactions predominate. Sharp (15) has recently provided evidence that this deterioration mechanism is active-carbonyl amine browning with glucose and phosphorylated sugars as the most important reactants. The recent work of Hendrickson et al. (,3, d ) on precooked dehydrated pork has shown that the browning reaction is probably an important factor in the storage deterioration, f o r the oxidation of glucose by glucose oxidase has a highly beneficial effect on the storage stability. This approach is apparently a valid analogy to similar studies of the storage deterioration of dehydrated eggs. The removal of glucose from eggs by fermentation by yeast or oxidation by glucose oxidase has been effectively used to decrease the deterioration of this product (10). The review by Coulter, Jenness, and Geddes ( 2 ) points up the importance of the browning reaction in the storage of dry milk. It therefore appears that the browning reaction could be one of the major, if not the most important non-oxidative deterioration mechanism in freeze-dried meat.It is the purpose of this research t o define the major physical and cheniical changes which occur during the storage deterioration of freezedried beef. On the basis of the changes found possible reaction mechanisms are analyzed. EXPERIMENTAL Preparation of material. Pieces of biceps fernoris of becf of about one-inch thickness were freeze-dried at a plate temperature of 40" C. and pressure of 0.1 mm. in a