Abstract:to study the dissipation behaviour of fipronil and its metabolites in clay soil under laboratory condition. In method verification, acetonitrile based extraction and dispersive clean-up approach adopted to quantify the residues of fipronil and its metabolites with gas chromatography (GC-ECD) from soil was accurate, precise and sensitive enough. The soils were spiked at the rate of 1.0 and 2.0 mg/kg level for single and double dose, respectively. Soil was extracted at 5, 10, 20, 30, 60, 90 and 120 days after in… Show more
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