Displacement of hydroxyl groups

Brown, Geoffrey W.

doi:10.1002/9780470771259.ch11

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1986

2002

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Cited by 9 publications

(1 citation statement)

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“…Incontrast, treatment of 4a with PBr3 gave 4b in 37% yield ( 7 ) . The chlorocompound 4c was obtained in 56% yield from 4a by treating with thionyl chloride and pyridine (8).…”

Section: Scheme Imentioning

confidence: 99%

Synthesis of 2,6‐dimethyl‐l,2,3,4‐tetrahydronaphthalene‐4‐¹³C and 2,6‐dimethylnaphthalene‐4¹³C

Bymaster

Pickering

Dobbs

et al. 1986

Labelled Comp Radiopharmac

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SUMMARYThe synthesis of specifically labeled 6,4-dimethyl-benzenebutanoic acid-l-C, 3,4-Dihydro-3,7-dirnethyl-l(2fJ)-naphthalen~ne-L-~~C, 2,6-dimethyl-l,2,3,4-tetrahydronaphthalene-4-13 C and Z,L-dimethylnaphthale~~e-i-'~c from Diethyl 2-(4-methylphenyl)-2-methylpropanediate is described. 13Key Words: 6,4-Dimethyl-benzenebutanoic acid-l-l3S, 3,4-dihydro-3,7-dimethyl-1 ( 2E) -napht ha 1 enone-l-3C, 2,6-d ime thy 1 -1 ,2 ,3,4-t e t r a hy d ronap h t ha 1 ene-4-3C and 2,6-dimethylnaphtha1ene-i-13c.

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“…Incontrast, treatment of 4a with PBr3 gave 4b in 37% yield ( 7 ) . The chlorocompound 4c was obtained in 56% yield from 4a by treating with thionyl chloride and pyridine (8).…”

Section: Scheme Imentioning

confidence: 99%