2H-NbSe 2 is one of the most widely researched transition metal dichalcogenide (TMD) superconductors, which undergoes charge-density wave (CDW) transition at T CDW about 33 K and superconducting transition at T c of 7.3 K. To explore the relation between its superconductivity and Fermi surface nesting, we combined S substitution with Cu intercalation in 2H-NbSe 2 to make Cu x NbSe 2-y S y (0 ≤ x = y ≤ 0.1).Upon systematic substitution of S and intercalation of Cu ions into 2H-NbSe 2 , we found that when the Cu and S contents (x = y 0.06) increases, the T c decreases in Cu x NbSe 2-y S y . While at higher x and y values, T c keeps a constant value near 2 K, which is not commonly observed for a layered TMD. For comparison, we found the simultaneous substitution of Nb by Cu and Se by S in Cu x Nb 1-x Se 2-y S y (0 ≤ x = y ≤ 0.06) lowered the T c substantially faster. We construct a superconducting phase diagrams for our double-doping compounds in contrast with the related single-ions doping systems.