2009
DOI: 10.1107/s1600536809037817
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Dichlorido(η4-cycloocta-1,5-diene)bis(triphenylphosphine)osmium(II)

Abstract: Key indicators: single-crystal X-ray study; T = 173 K; mean (C-C) = 0.008 Å; R factor = 0.022; wR factor = 0.044; data-to-parameter ratio = 12.5.The Os II atom in the title compound, [OsCl 2 (C 8 H 12 )-(C 18 H 15 P) 2 ], is located on a crystallographic twofold axis and adopts a distorted octahedral coordination geometry. The two triphenylphosphine ligands are trans to each other, while the two chlorine ligands are cis-disposed. The coordination is completed by the cyclooctadiene (COD) ligand with bonding to … Show more

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