2012
DOI: 10.2465/jmps.110520
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Development of a fully automated open-column chemical-separation system—COLUMNSPIDER—and its application to Sr-Nd-Pb isotope analyses of igneous rock samples

Abstract: A fully automated open -column resin -bed chemical -separation system, named COLUMNSPIDER, has been developed. The system consists of a programmable micropipetting robot that dispenses chemical reagents and sample solutions into an open -column resin bed for elemental separation. After the initial set up of resin columns, chemical reagents, and beakers for the separated chemical components, all separation procedures are automated. As many as ten samples can be eluted in parallel in a single automated run. Many… Show more

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Cited by 21 publications
(20 citation statements)
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References 53 publications
(61 reference statements)
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“…The analytical results for the groundmass of the SH35 sample showed excellent agreement with the bulk-rock composition analysed by solution MC-ICP-MS (Miyazaki et al, 2012) (Fig. 5B).…”
Section: Silicate Mineralssupporting
confidence: 64%
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“…The analytical results for the groundmass of the SH35 sample showed excellent agreement with the bulk-rock composition analysed by solution MC-ICP-MS (Miyazaki et al, 2012) (Fig. 5B).…”
Section: Silicate Mineralssupporting
confidence: 64%
“…For comparison with bulk-rock Pb isotope compositions, basalt lava samples from Pitcairn Island (PC samples) were analysed by solution MC-ICP-MS using an Aridus desolvating nebulizer and a Neptune MC-ICP-MS (Thermo Fisher, Bremen, Germany) with normal samples, and skimmer cones after the Pb separation procedure (Miyazaki et al, 2012).…”
Section: Mc-icp-msmentioning
confidence: 99%
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“…The analytical procedure used for the chemical separation and mass spectrometry for Sr and Nd isotope determinations is outlined in Hirahara et al (2009), and Miyazaki et al (2012. Total procedural blanks for Sr and Nd during the measurement period were less than 177 pg and 5 pg, respectively.…”
Section: Analytical Techniquesmentioning
confidence: 99%
“…The analytical procedures for the isotopic ratios included chemical separation and mass spectrometry, following the methods reported previously for Sr, Nd, and Pb isotopes [ Hirahara et al ., ; Miyazaki et al ., ; Takahashi et al ., ]. Isotopic ratios of Sr and Nd were determined by using a thermal ionization mass spectrometer (Triton TI; Thermo Fisher Scientific, Bremen, Germany), with fractionation correction by using 86 Sr/ 88 Sr = 0.1194 and 146 Nd/ 144 Nd = 0.7219, respectively.…”
Section: Samples and Analyticalmentioning
confidence: 99%