Development of 3H, 14C, 41Ca, 55Fe, 63Ni radiochemical analysis methods in activated concrete samples

Abstract

Development of 3H, 14C, 41Ca, 55Fe and 63Ni radiochemical analysis methods were carried out independently by two laboratories using both inactivate and activated concrete samples. Two preliminary radioanalytical procedures for the non-volatile radionuclides (41Ca, 55Fe, 63Ni) and one Thermal oxidation method for the volatile radionuclides (3H, 14C) were developed. The difficulties in the method development and analysis of results are discussed.