Determination of the Bone Mineral Crystallite Size and Lattice Strain from Diffraction Line Broadening

Danilchenko, S. N.; Kukharenko, O.; Moseke, Claus; Protsenko, І. Yu.; Sukhodub, L. F.; Sulkio-Cleff, B.

doi:10.1002/1521-4079(200211)37:11<1234::aid-crat1234>3.0.co;2-x

Cited by 177 publications

(97 citation statements)

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“…This allowed to calculate the values of L and e with accuracy of about 30-50% [22,23]. In order to provide more precise calculations of L and e values with the accuracy of about 11-16% the three-fold convolution method was used [24,25].…”

Section: Methodssupporting

confidence: 62%

Study of the structural and photoluminescence properties of CdTe polycrystalline films deposited by close-spaced vacuum sublimation

Kosyak

Opanasyuk

Bukivskij

et al. 2010

Journal of Crystal Growth

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a b s t r a c tThe polycrystalline CdTe films were deposited by the close-spaced vacuum evaporation at the different substrate temperatures (150-550 1C). The X-ray diffraction measurements of structural and substructural properties of these films were carried out to study their phase composition and texture. The films' parameters such as the coherent scattering domain size, microdeformation level and mean density of dislocations were determined based on the broadening of diffraction peaks. In this case the Hall and three-fold convolution approximations were used. Surface morphology, grain size and growth mechanism of the films were determined by the scanning electron microscopy. The low temperature photoluminescence measurements allowed us to establish the correlation between the point and extended defect structure on the one hand and the growth conditions on the other. As a result, the growth conditions of CdTe polycrystalline films with fairly good crystal and optical quality were determined.

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Section: Methodssupporting

confidence: 62%

Study of the structural and photoluminescence properties of CdTe polycrystalline films deposited by close-spaced vacuum sublimation

Kosyak

Opanasyuk

Bukivskij

et al. 2010

Journal of Crystal Growth

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“…The average values for the crystallite sizes are ~20.1 nm, ~20.4 nm, and ~20.8 nm for the spinous process, lateral processes, and spine base, respectively. These crystallite sizes are similar to that of bovine femur bone [50]. It is of note that while other fish scales have been known to contain calcite as mentioned in Section 2.2.3, no calcite was found in the porcupine fish spines.…”

Section: X-ray Diffractionsupporting

confidence: 74%

Spines of the porcupine fish: Structure, composition, and mechanical properties

Bushong

Deerinck

et al. 2017

Journal of the Mechanical Behavior of Biomedical Materials

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“…Figure 1 The crystalline sizes of the synthesized Gel-HAP were calculated from the observed XRD patterns using the Debye-Scherer equation [37][38]. Calculated particle sizes (in nm) for the various gelatin concentrations, ultrasonic power and temperatures are tabulated in Table 1.…”

Section: Resultsmentioning

confidence: 99%

Effect of dilute gelatine on the ultrasonic thermally assisted synthesis of nano hydroxyapatite

Brundavanam

Jiang

Chapman

et al. 2011

Ultrasonics Sonochemistry

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Accepted ManuscriptThis is a PDF file of an unedited manuscript that has been accepted for publication. As a service to our customers we are providing this early version of the manuscript. The manuscript will undergo copyediting, typesetting, and review of the resulting proof before it is published in its final form. Please note that during the production process errors may be discovered which could affect the content, and all legal disclaimers that apply to the journal pertain. Effect of Dilute Gelatine on the Ultrasonic Thermally AbstractA series of nano hydroxyapatite-gelatin composites with different dilute solutions of gelatin concentrations were synthesized by a thermally assisted low power ultrasonic irradiation method.The gelatine hydroxyapatite, (Gel-HAP) nanoparticles were prepared using Ca(NO 3 ) 2 and KH 2 PO 4 in the presence of gelatine in an aqueous solution. The synthesised products were heat treated between 100°C and 400°C. The effect of the addition of gelatin on the nucleation and growth of synthesised nano HAP was investigated. Characterisation was performed using X-ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM) and Fourier transform infrared spectroscopy (FT-IR). The characterisation results indicate that gelatin has been appended to the nano HAP forming regular spherical shaped crystals of nano sized Gel-HAP.

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Determination of the Bone Mineral Crystallite Size and Lattice Strain from Diffraction Line Broadening

Cited by 177 publications

References 0 publications

Study of the structural and photoluminescence properties of CdTe polycrystalline films deposited by close-spaced vacuum sublimation

Study of the structural and photoluminescence properties of CdTe polycrystalline films deposited by close-spaced vacuum sublimation

Spines of the porcupine fish: Structure, composition, and mechanical properties

Effect of dilute gelatine on the ultrasonic thermally assisted synthesis of nano hydroxyapatite

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