Determination of oxprenolol, methandienone and testosterone in meat samples by UHPLC-Q-ToF

Темердашев, А. З.; Dmitrieva, Ekaterina; Azaryan, A. A.; Gashimova, Elina

doi:10.1016/j.heliyon.2023.e13260

Cited by 6 publications

(4 citation statements)

References 37 publications

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“…The LODs and LOQs for the twelve AASs were evaluated by testing a series of concentrations of spiked blank samples. The spiked concentration at S/N ≥ 3 was used as the LOD of the method, and the spiked concentration at S/N ≥ 10 was used as the LOQ of the method [ 43 ].…”

Section: Methodsmentioning

confidence: 99%

Rapid and Simultaneous Determination of Anabolic Andro-Genic Steroids in Livestock and Poultry Meat Using One-Step Solid-Phase Extraction Coupled with UHPLC–MS/MS

Wang,

Yan,

Wang

et al. 2023

Molecules

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Anabolic androgenic steroids (AASs) are usually illegally added to animal feed because they can significantly promote animal growth and increase carcasses’ leanness, which threatens the safety of animal-derived foods and indirectly hazards human health. This study aimed to establish an ultra-high performance liquid chromatography-tandem mass spectrometry (UHPLC–MS/MS) method for the simultaneous detection of twelve AAS residues in livestock and poultry meat. The homogenized samples were extracted with acetonitrile containing 1% acetic acid (v/v) and purified using the one-step extraction column. After concentration using nitrogen, the residues were redissolved in acetonitrile and then quantified with an external standard method using UHPLC–MS/MS. The results showed that the above-mentioned method had a satisfactory linear correlation (R2 ≥ 0.9903) with a concentration range of 1–100 μg/L, and the limits of detection (LODs) and quantification (LOQs) were 0.03–0.33 μg/kg and 0.09–0.90 μg/kg, respectively. With the intraday and interday precision less than 15%, the average recoveries of pork, beef, lamb, and chicken, at different spiked levels, ranged from 68.3 to 93.3%, 68.0 to 99.4%, 71.6 to 109.8%, and 70.5 to 97.7%, respectively. Overall, the established method is validated, precise, and capable of the high-throughput determination of the residues of twelve AASs in livestock and poultry meat.

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Section: Methodsmentioning

confidence: 99%

Rapid and Simultaneous Determination of Anabolic Andro-Genic Steroids in Livestock and Poultry Meat Using One-Step Solid-Phase Extraction Coupled with UHPLC–MS/MS

Wang,

Yan,

Wang

et al. 2023

Molecules

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“…The sensor can be installed on the desktop or wall to sense and locate external vibration sources. Apart from surface-to-surface contact based on contact and separation mode TENG, ball-in-tube structure sensor have also been reported by Peng et.al, [50] which could function as a self-powered vibration speed sensor within the range from 0.3 to 1.5 m s −1 . More recently, researchers have started to apply mechanical vibration sensors in practical use, for example a magnetic -assisted self-powered acceleration sensor (MSAS) based on the triboelectric nanogenerator has been proposed as demonstrated in Figure 8c, to monitor low acceleration under normal operation [45] Copyright 2022, Elsevier.…”

Section: Mechanical Vibration Sensormentioning

confidence: 99%

Advances in Multifunctional Sensors Based on Triboelectric Nanogenerator – Applications, Triboelectric Materials, and Manufacturing Integration

Liao,

Ni,

Peng

et al. 2024

Adv Materials Technologies

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With the rapid development of industry and information technology, rough challenges have been put forward for the traditional sensor technology to meet the increasingly complex and diverse application demands in actual production and daily life, and the widely distributed sensor network also faces complex power supply and maintenance problems. As a new energy conversion technology, triboelectric nanogenerators (TENGs) based on triboelectrification and electrostatic induction effect can respond to the weak mechanical stimuli in the surrounding environment and generate corresponding electrical signals to realize the sensing function without external power supply. In addition, TENGs have the advantages of wide selection of fabrication materials, flexible and diverse fundamental modes, which can be customized for different applications and realize different sensing functions. In recent years, triboelectric sensors based on TENGs have developed rapidly, and researchers have developed variable triboelectric sensors for different application scenarios. In this paper, the developed triboelectric sensos have been classified into different categories, the advanced strategy to prepare advanced triboelectric materials and technology used for manufacturing integration have been introduced. This work summarizes the main applications of triboelectric sensors and put forward the current challenges, so as to provide guidance and instructions for the future development of triboelectric sensors.

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“…In addition, SPE can also increase sensitivity to a higher level. A study conducted by Temerdashev et al in 2023 reported that the use of SPE with HLB cartridges in meat samples was suitable for the quantitative separation of methandionone, oxprenolol, and testosterone with high sensitivity, accuracy and precision [ 39 ].…”

Section: Drug Residues In Foodmentioning

confidence: 99%

“…Recently, Temerdashev et al (2023) determined Oxprenolol, methandienone and testosterone in meat samples with UHPLC-Q-TOF-MS method [39]. Q-TOF-MS offers high sensitivity and mass accuracy for both precursor and product ions, enabling rapid elemental composition confirmation.…”

Section: Chromatographic Techniquementioning

confidence: 99%

Recent Advances in the Determination of Veterinary Drug Residues in Food

Pratiwi,

Ramadhanti,

Amatulloh

et al. 2023

Foods

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The presence of drug residues in food products has become a growing concern because of the adverse health risks and regulatory implications. Drug residues in food refer to the presence of pharmaceutical compounds or their metabolites in products such as meat, fish, eggs, poultry and ready-to-eat foods, which are intended for human consumption. These residues can come from the use of drugs in the field of veterinary medicine, such as antibiotics, antiparasitic agents, growth promoters and other veterinary drugs given to livestock and aquaculture with the aim of providing them as prophylaxis, therapy and for promoting growth. Various analytical techniques are used for this purpose to control the maximum residue limit. Compliance with the maximum residue limit is very important for food manufacturers according to the Food and Drug Administration (FDA) or European Union (EU) regulations. Effective monitoring and control of drug residues in food requires continuous advances in analytical techniques. Few studies have been reviewed on sample extraction and preparation techniques as well as challenges and future directions for the determination of veterinary drug residues in food. This current review focuses on the overview of regulations, classifications and types of food, as well as the latest analytical methods that have been used in recent years (2020–2023) for the determination of drug residues in food so that appropriate methods and accurate results can be used. The results show that chromatography is still a widely used technique for the determination of drug residue in food. Other approaches have been developed including immunoassay, biosensors, electrophoresis and molecular-based methods. This review provides a new development method that has been used to control veterinary drug residue limit in food.

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Determination of oxprenolol, methandienone and testosterone in meat samples by UHPLC-Q-ToF

Cited by 6 publications

References 37 publications

Rapid and Simultaneous Determination of Anabolic Andro-Genic Steroids in Livestock and Poultry Meat Using One-Step Solid-Phase Extraction Coupled with UHPLC–MS/MS

Rapid and Simultaneous Determination of Anabolic Andro-Genic Steroids in Livestock and Poultry Meat Using One-Step Solid-Phase Extraction Coupled with UHPLC–MS/MS

Advances in Multifunctional Sensors Based on Triboelectric Nanogenerator – Applications, Triboelectric Materials, and Manufacturing Integration

Recent Advances in the Determination of Veterinary Drug Residues in Food

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