Determination of nitrofuran metabolites in shrimp by high performance liquid chromatography with fluorescence detection and liquid chromatography–tandem mass spectrometry using a new derivatization reagent

Du, Nana; Chen, Mingming; Lei, Sheng; Chen, Shui-Sheng; Xu, Huajie; Liu, Zhao‐Di; Song, Chenyu; Qiao, Rui

doi:10.1016/j.chroma.2013.12.065

Cited by 71 publications

(38 citation statements)

References 37 publications

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“…Consequently, rapid and sensitive analytical methods for NFZ are required, particularly in the fields of bioassay and chemistry. In this context many methods have been developed: spectrophotometry [34], chromatography [35], high performance liquid chromatography (HPLC) with fluorescence detection (HPLC-FLD) [36], voltammetry [30], FI-CL method [37] and fluorescence [38].…”

Section: Introductionmentioning

confidence: 99%

The use of tungsten disulfide dots as highly selective, fluorescent probes for analysis of nitrofurazone

Guo

Wang

et al. 2015

Talanta

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Section: Introductionmentioning

confidence: 99%

The use of tungsten disulfide dots as highly selective, fluorescent probes for analysis of nitrofurazone

Guo

Wang

et al. 2015

Talanta

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“…Several methods describe the assessment of nitrofuran metabolite concentrations in substances, including gas chromatography (Negrin, Valdes, Pouron, Lopez, & Borges, 2013;Petz, 1985), high performance liquid chromatography (Fernando, Munasinghe, Gunasena, & Abeynayake, 2017;Li, Ren, et al, 2018;Sniegocki, Giergiel, Sell, & Posyniak, 2018;Wilasinee, Sutthivaiyakit, & Sutthivaiyakit, 2015), and liquid chromatography tandem mass spectrometry (Du et al, 2014;El-Demerdash, Song, Reel, Hillegas, & Smith, 2015;Palaniyappan et al, 2013). Similarly, few studies have reported NFS determination using high-performance liquid chromatography and/or liquid chromatography tandem mass spectrometry (Horie et al, 1991;Segawa & Ikeda, 2000;Tao et al, 2010).…”

Section: Introductionmentioning

confidence: 99%

Development of an immunochromatographic strip test for rapid detection of sodium nifurstyrenate in fish

Song

Suryoprabowo

Liu

et al. 2019

Food and Agricultural Immunology

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A rapid, specific and sensitive method based an immunochromatographic strip test has been developed for the determination of sodium nifurstyrenate (NFS) residues in fish. Sample preparation procedure includes ultrasonic bath extraction with acetonitrile, sample centrifugation at 8000 rpm for 10 min, filtration through the 0.22 µm membrane filter, and drying over nitrogen (60°C) and res-suspension. The antigen (NFS-ovalbumin) and a goat anti-mouse IgG antibody were drawn onto a nitrocellulose membrane as the test line and control line, respectively. Under optimized conditions, the NFS cutoff limits for test strips was determined as 5 ng/mL in 0.01 M phosphate buffered saline and 10 ng/mL in fish. Results were obtained within 5 min. Our data suggests this immunochromatographic assay can be used for the sensitive, rapid, and specific on-site screening for NFS in fish.

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“…Semicarbazide (SEM) is a hydrazine derivative and widely exists in food as a toxic contaminant with carcinogenicity, teratogenicity, mutagenicity, and other side effect. Some previous reports suggested that the rapidly screening SEM could provide crucial clues for the evaluation for illegal abuse of veterinary drug of nitrofurazone . Moreover, the evidence in literatures showed that SEM could not only be detected in food packed in glass jars and bottles with plastic gaskets using azodicarbonamide as foaming agent, but also presented in food using ADC as gluten fortifier .…”

Section: Introductionmentioning

confidence: 99%

Rapid determination of trace semicarbazide in flour products by high‐performance liquid chromatography based on a nucleophilic substitution reaction

Wei

Zhang

2017

J of Separation Science

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Semicarbazide, a toxic food contaminant, widely exists in food products and it originates from the thermal degradation of a food additive of azodicarbonamide or a metabolite of nitrofurazone abused in meat specimens. Many previous methods for semicarbazide determination usually required expensive instruments, difficult-to-prepare monoclonal antibodies, and a long operation time. In this study, a high-performance liquid chromatography method was developed for the rapid determination of trace semicarbazide coupling with a nucleophilic substitution reaction firstly using 4-nitrobenzoyl chloride as derivatization reagent. The derivatization reaction was mild at room temperature for 1 min in neutral solution. Then, semicarbazide derivative was separated and quantified by high-performance liquid chromatography with ultraviolet detection under optimal separation conditions at λ = 261 nm. The proposed method offered the detection limit of 1.8 μg/L and was successfully applied for the rapid determination of trace semicarbazide in flour products. Semicarbazide in positive real samples could be actually found and quantified in the range of 0.47-7.53 mg/kg. The recoveries were 76.6-119% with relative standard deviations of 0.5-9.1% (n = 3). This developed method was rapid, reliable, and convenient for the determination of trace semicarbazide in food.

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Determination of nitrofuran metabolites in shrimp by high performance liquid chromatography with fluorescence detection and liquid chromatography–tandem mass spectrometry using a new derivatization reagent

Cited by 71 publications

References 37 publications

The use of tungsten disulfide dots as highly selective, fluorescent probes for analysis of nitrofurazone

The use of tungsten disulfide dots as highly selective, fluorescent probes for analysis of nitrofurazone

Development of an immunochromatographic strip test for rapid detection of sodium nifurstyrenate in fish

Rapid determination of trace semicarbazide in flour products by high‐performance liquid chromatography based on a nucleophilic substitution reaction

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