2008
DOI: 10.1080/03067310802308483
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Determination of mineral and trace element concentrations in pine needles by ICP-OES: evaluation of different sample pre-treatment methods

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Cited by 21 publications
(6 citation statements)
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“…The digestate and feedstock samples for the trace element analysis (III) were first dried (24 h, 105 °C), milled in a rotor mill (Pulverisette 14, Fritsch, Germany) and stored at 22 °C until analysed. The concentration of the trace elements was measured using a Perkin-Elmer (Norwalk, CT, USA) Optima 4300 DV ICP-OES using the following default parameters of the instrument: nebulizer flow 0.5-1.0 l min -1 , auxiliary gas flow 0.2 l min -1 , plasma gas flow 15 l min -1 and plasma power of 1300 or 1400 W (Väisänen et al 2008). …”
Section: Post-methanation Assays (Iii Iv)mentioning
confidence: 99%
“…The digestate and feedstock samples for the trace element analysis (III) were first dried (24 h, 105 °C), milled in a rotor mill (Pulverisette 14, Fritsch, Germany) and stored at 22 °C until analysed. The concentration of the trace elements was measured using a Perkin-Elmer (Norwalk, CT, USA) Optima 4300 DV ICP-OES using the following default parameters of the instrument: nebulizer flow 0.5-1.0 l min -1 , auxiliary gas flow 0.2 l min -1 , plasma gas flow 15 l min -1 and plasma power of 1300 or 1400 W (Väisänen et al 2008). …”
Section: Post-methanation Assays (Iii Iv)mentioning
confidence: 99%
“…Subsamples of freshly collected leaves and leached preconditioned leaves were lyophilised, ground to fine powder in a ball mill and analysed for contents of total carbon and nitrogen (Elementar vario EL C/N elemental analyser, Hanau, Germany), fibrous compounds (gravimetric determination of acid detergent lignin and cellulose, Gessner et al ., ), and phenols (detection with a spectrophotometer following extraction with 70% acetone and addition of Folin‐Cialteau reagent, Bärlocher & Graça, ). Furthermore, concentrations of Ca, Mg, K and P were determined by ignition (4 h at 450 °C) followed by extraction with 10 mL of aqua regia:ultrapure water (1:1) solution in an ultrasonic bath (Väisänen et al ., ) and detection with an ICP‐OE spectrometer (Thermo Scientific, iCAP 6500, USA, wavelengths: Ca 318.1 nm axial, K 766.4 nm axial; Mg 285.2 nm axial, P 214.9 nm radial).…”
Section: Methodsmentioning
confidence: 99%
“…Thus the analytical methods applied will be described more detailed here. Since the early 1980s the underlying general methods have been proven to be suitable for various plant matrixes (e.g., Vaisanen et al 2008).…”
Section: Chemical Leaf Analysismentioning
confidence: 99%