2014
DOI: 10.1007/s11340-014-9877-z
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Determination of Local Thermophysical Properties and Heat of Transition from Thermal Fields Measurement During Drop Calorimetric Experiment

Abstract: This paper proposes a non-contact original method to estimate local thermophysical properties (heat capacity and thermal conductivity) and heats of transition from plane thin specimens. This method is based on measurement of temperature fields with an infrared camera during a drop calorimetric experiment. A studied specimen and a reference specimen, with similar geometries, are simultaneously tested. Firstly, the method is validated by estimating heat capacity and thermal conductivity of Vanadium specimens and… Show more

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Cited by 13 publications
(11 citation statements)
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“…The application to rubber is typical of the relevance of the approach in studying various material responses: [12][13][14][15][16][17] thermoelastic coupling, entropic coupling, thermoelastic inversion, the effect of reinforcement by fillers, strain-induced crystallization, and the Mullins effect. The 0D approach has been also applied to study the thermomechanical response of SMAs under cyclic loading, [7,[18][19][20][21][22] as well as polyamide 6.6, [23][24][25][26][27] aluminum alloy, [28] and steel. [29] However, a difficulty arises for the estimation of mechanical dissipation in the case of long-term cyclic tests: The results are easily skewed by any change in the specimen's environment, such as the ambient air, the grips of the testing machine, and more generally, all the components of the testing room.…”
Section: Introductionmentioning
confidence: 99%
“…The application to rubber is typical of the relevance of the approach in studying various material responses: [12][13][14][15][16][17] thermoelastic coupling, entropic coupling, thermoelastic inversion, the effect of reinforcement by fillers, strain-induced crystallization, and the Mullins effect. The 0D approach has been also applied to study the thermomechanical response of SMAs under cyclic loading, [7,[18][19][20][21][22] as well as polyamide 6.6, [23][24][25][26][27] aluminum alloy, [28] and steel. [29] However, a difficulty arises for the estimation of mechanical dissipation in the case of long-term cyclic tests: The results are easily skewed by any change in the specimen's environment, such as the ambient air, the grips of the testing machine, and more generally, all the components of the testing room.…”
Section: Introductionmentioning
confidence: 99%
“…This case is similar to the exothermic heat source that occurs during a thermal induced phase transformation, as in the experimental benchmarks proposed in [15,20]. In [15,20], the NiTi SMA cools from a high temperature where the material is in • Case 2: Fig. 3.b were chosen.…”
Section: Methodsmentioning
confidence: 99%
“…The second one, qualified as "experimental" refers to real problems where temperature and heat sources are quantitatively known. [15,20] proposed a first experimental vali-dation based on the observation of the austenite to R phase transformation occurring in NiTi SMA.…”
Section: Introductionmentioning
confidence: 99%
“…For this purpose, temperature fields are acquired using an infrared thermal camera. This method for heat source quantification using infrared technique was validated by authors in [19,20,21] in a NiTi tube and plate showing typical DSC results, i.e. well-defined transformation peaks.…”
Section: Introductionmentioning
confidence: 96%