Determination of ethylphenol compounds in wine by headspace solid-phase microextraction in conjunction with gas chromatography and flame ionization detection

Abstract

headspace solid-phase microextraction in conjunction with gas chromatography and flame ionization detection. (2002) Analytica Chimica Acta, 458 (1). 111-117.

Solid-Phase Microextraction (SPME) Techniques for Quality Characterization of Food Products: A Review

“…The use of SPME for the extraction of volatile organic compounds from alcoholic beverages, particularly wine, is well-documented (Hayasaka and Bartowsky 1999;Rocha et al 2001;Azenha and Vasconcelos 2002;Hartmann et al 2002;Monje et al 2002;Rodriguez-Bencomo et al 2003). Different fiber coatings (PA, PDMS, DVB/PDMS, DVB/ CARB/PDMS, and Carbowax/DVB) have been found to extract volatiles from wines satisfactorily (Table 2).…”

A Case Study of Selected Volatile Phenols from Brettanomyces and Micronutrients Mn, Fe, Cu, Zn in Chianti Red Wines

“…The procedure was optimized via trial and error method on standard solutions, by starting from previous reports (Monje, 2002;Pizarro, 2007) and the guide lines from the producer (Sigma-Aldrich Co. Supelco, 2010) according to the available instruments (see just below) and to results from external private laboratory. The fiber for SPME was a polyacrylate one, 85 μm (Supelco, Milan, Italy).…”

Quantitative analysis of 2-furfural and 5-methylfurfural in different Italian vinegars by headspace solid-phase microextraction coupled to gas chromatography–mass spectrometry using isotope dilution

“…This technique has been successfully applied in combination with GC and HPLC to the determination of a wide variety of analytes from environmental [11,12], biological [13] and food [14][15][16][17][18][19][20][21] samples.…”