Determination of Cefoperazone Sodium in Pharmaceutical Formulations by Fe3+-Phenanthroline Spectrophotometry

Sha, Ou; Yin, Lin; Zhou, Yun; Zhang, Si Liang; Wei-xing, MA

doi:10.14233/ajchem.2013.14204

Asian J. Chem.

2013

DOI: 10.14233/ajchem.2013.14204

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Determination of Cefoperazone Sodium in Pharmaceutical Formulations by Fe3+-Phenanthroline Spectrophotometry

Ou Sha¹,

Lin Yin²,

Yun Zhou³

et al.

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Cited by 2 publications

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“…Various analytical methods are applied for the determination of cefoperazone. These methods include spectrophotometry (Hoang et al, 2014;Sha et al, 2013) and HPLC (Lalitha, Puranik, Pai, 2009).…”

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confidence: 99%

Determination of cefotaxime, cefoperazone, ceftazidime and cefadroxil using surface plasmon resonance band of silver nanoparticles

Salem

Samir

2018

Braz. J. Pharm. Sci.

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The aim of this work is to evaluate simple, sensitive, effective and validated procedures for the determination of cefotaxime, cefoperazone, ceftazidime and cefadroxil. In this study, the methods based on the ability of the cited drugs to reduce Ag + ions to silver nanoparticles (Ag-NPs) in the presence of Polyvinyl Pyrrolidone (PVP) as a stabilizing agent producing very intense surface plasmon resonance peak of Ag-NPs (λ max. = 410-430 nm). The plasmon absorbance of the Ag-NPs allows the quantitative spectrophotometric determination of the cited drugs. The calibration curves are linear with concentration ranges of 0.4-3.2, 1-8, 0.5-4.0 and 1.5-9.0 µg/mL for cefotaxime, cefoperazone, ceftazidime and cefadroxil, respectively. Apparent molar absorptivity, detection and quantitative limits are calculated. Applications of the proposed methods to representative pharmaceutical formulations are successfully presented. The extracellular synthesis of nanoparticles is fast, and the method doesn ' t require various elaborate treatments and tedious extraction procedures.

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confidence: 99%

Determination of cefotaxime, cefoperazone, ceftazidime and cefadroxil using surface plasmon resonance band of silver nanoparticles

Salem

Samir

2018

Braz. J. Pharm. Sci.

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Flow Injection Analysis (FIA) with Thermal Lens Spectrometry (TLS) for the Rapid Determination of Cefoperazone in Urine and Water

et al. 2022

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Determination of Cefoperazone Sodium in Pharmaceutical Formulations by Fe3+-Phenanthroline Spectrophotometry

Cited by 2 publications

References 15 publications

Determination of cefotaxime, cefoperazone, ceftazidime and cefadroxil using surface plasmon resonance band of silver nanoparticles

Determination of cefotaxime, cefoperazone, ceftazidime and cefadroxil using surface plasmon resonance band of silver nanoparticles

Flow Injection Analysis (FIA) with Thermal Lens Spectrometry (TLS) for the Rapid Determination of Cefoperazone in Urine and Water

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