Determination of biogenic amines in canned fish samples using head-space solid phase microextraction based on nanostructured polypyrrole fiber coupled to modified ionization region ion mobility spectrometry

Parchami, Razieh; Kamalabadi, Mahdie; Alizadeh, Naader

doi:10.1016/j.chroma.2016.12.046

Cited by 45 publications

(21 citation statements)

References 37 publications

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“…Lower peak intensities were evident in the pH range from 2 to 6, while peak intensities increased for the pH range 8 to 12. This is due to the suppression of dissociation of BAs in alkaline conditions to the non-ionic form [19]. Peak intensities compared to pH value is given in Fig.…”

Section: Phmentioning

confidence: 98%

Direct solid phase microextraction combined with gas chromatography – Mass spectrometry for the determination of biogenic amines in wine

Papageorgiou

Lambropoulou

Morrison

et al. 2018

Talanta

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A direct method based on immersion solid phase microextraction (DI-SPME) gas chromatography mass-spectrometry (GC-MS) was optimized and validated for the determination of 16 biogenic amines in Polish wines. In the analysis two internal standards were used: 1,7-diaminoheptane and bis-3-aminopropylamine. The method allows for simultaneous extraction and derivatization, providing a simple and fast mode of extraction and enrichment. Different parameters which affect the extraction procedure were studied and optimized including ionic strength (0-25%), fiber materials (PDMS/DVB, PDMS/DVD + OC, Polyacrylate, Carboxen/PDMS and DVB/CAR/PDMS) and timings of the extraction, derivatization and desorption processes. Validation studies confirmed the linearity, sensitivity, precision and accuracy of the method. The method was successfully applied to the analysis of 44 wine samples originating from several regions of Poland and 3 wine samples from other countries. Analysis showed that many of the samples contained all examined biogenic amines. The method, assessed using an Eco-Scale tool with satisfactory results, was found to be green in terms of hazardous chemicals and solvents usage, energy consumption and production of waste. Therefore the proposed method can be safely used in the wine industry for routine analysis of BAs in wine samples with a minimal detrimental impact on human health and the environment.

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Section: Phmentioning

confidence: 98%

Direct solid phase microextraction combined with gas chromatography – Mass spectrometry for the determination of biogenic amines in wine

Papageorgiou

Lambropoulou

Morrison

et al. 2018

Talanta

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“…Actually, a chemical derivatization is mandatory to allow the sensitive determination of PAs by spectroscopic techniques, as their molecular structure lacks of moieties with optical or fluorescent properties (Al-Hadithi and Saad 2011). In addition, thin layer chromatography (Lapa-Guimarães and Pickova 2004), ion mobility spectrometry (Parchami et al 2017), NMR (Shumilina et al 2016) and colorimetric methods (Morsy et al 2016), were also proposed.…”

Section: Methods For the Determination Of Polyaminesmentioning

confidence: 99%

Endogenous and food-derived polyamines: determination by electrochemical sensing

et al. 2018

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Polyamines (PAs) are involved in a variety of fundamental physio-pathologic processes. The concentration of these polycations in organs and tissues depends on their endogenous production and oxidation rates, and on their intake from foods. Besides being largely accepted as markers for the progress of several pathologies, PAs may exert themselves different effects on humans, ranging from being positive to be drastically detrimental depending on the organism conditions. Thus, if the determination of polyamines content in tissue samples is of great importance as they could be indicators of several diseases, their quantification in food is fundamental for modulating the diet to respond to a specific human health status. Thus, the determination of PA content in food is increasingly urgent. Standard analytical methods for polyamine quantification are mainly based on chromatography, where high-performance liquid chromatography and gas chromatography are the most often used, involving pre-column or post-column derivatization techniques. Driven by the growing need for rapid in situ analyses, electrochemical biosensors, comprising various combinations of different enzymes or nanomaterials for the selective bio-recognition and detection, are emerging as competitors of standard detection systems. The present review is aimed at providing an up-to-date overview on the recent progresses in the development of sensors and biosensors for the detection of polyamines in human tissues and food samples. Basic principles of different electrochemical (bio)sensor formats are reported and the applications in human tissues and in foods was evidenced.

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“…Various methods to analysis of BAs have been developed such as high-performance liquid chromatography (HPLC) (Kaniou et al 2001), gas chromatography-mass spectrometry (GC-MS) (Almeida et al 2012;Park et al 2013), and ion mobility spectrometry (IMS) (Hashemian et al 2010;Parchami et al 2017;Karpas et al 2002a, b). Each of these analytical methods has advantages and disadvantages.…”

Section: Introductionmentioning

confidence: 99%

Determination of Histamine and Tyramine in Canned Fish Samples by Headspace Solid-Phase Microextraction Based on a Nanostructured Polypyrrole Fiber Followed by Ion Mobility Spectrometry

2017

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This paper describes the development of a simple, rapid, and selective method based on headspace solid-phase microextraction (HS-SPME) combined with ion mobility spectrometry (IMS) for the simultaneous determination of histamine (HIS) and tyramine (TYR) in the canned fish samples. The spectra interferences were eliminated by using a new alternate reagent gas and resulted in an increased sensitivity and selectivity of IMS technique. A dodecylbenzenesulfonate-doped polypyrrole coating was used as a fiber for HS-SPME method. The calibration curves were linear in the range of 30-300 ng g −1 (R 2 > 0.994). Limits of detection for HIS and TYR were 3 and 4 ng g −1 , respectively. The proposed method was successfully applied to determine HIS and TYR in different canned fish samples without derivatization steps. Method validation was conducted by comparing our results with those obtained through gas chromatographymass spectrometry method.

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Determination of biogenic amines in canned fish samples using head-space solid phase microextraction based on nanostructured polypyrrole fiber coupled to modified ionization region ion mobility spectrometry

Cited by 45 publications

References 37 publications

Direct solid phase microextraction combined with gas chromatography – Mass spectrometry for the determination of biogenic amines in wine

Direct solid phase microextraction combined with gas chromatography – Mass spectrometry for the determination of biogenic amines in wine

Endogenous and food-derived polyamines: determination by electrochemical sensing

Determination of Histamine and Tyramine in Canned Fish Samples by Headspace Solid-Phase Microextraction Based on a Nanostructured Polypyrrole Fiber Followed by Ion Mobility Spectrometry

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