2021
DOI: 10.3390/molecules26071837
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Determination of 77 Multiclass Pesticides and Their Metabolitesin Capsicum and Tomato Using GC-MS/MS and LC-MS/MS

Abstract: A quick, sensitive, and reproducible analytical method for the determination of 77 multiclass pesticides and their metabolites in Capsicum and tomato by gas and liquid chromatography tandem mass spectrometry was standardized and validated. The limit of detection of 0.19 to 10.91 and limit of quantification of 0.63 to 36.34 µg·kg−1 for Capsicum and 0.10 to 9.55 µg·kg−1 (LOD) and 0.35 to 33.43 µg·kg−1 (LOQ) for tomato. The method involves extraction of sample with acetonitrile, purification by dispersive solid p… Show more

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Cited by 10 publications
(6 citation statements)
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“…Rathod et al [ 11 ] validated a method for the determination of 77 multiclass pesticides and their metabolites in Capsicum and tomato by gas and liquid chromatography tandem mass spectrometry. The method that involved extraction and purification by a modified QuEChERS approach provided high accuracy, precision, reproducibility and ruggedness, detecting and quantifying pesticide residues below their prescribed EU and FSSAI MRLs.…”
Section: Resultsmentioning
confidence: 99%
“…Rathod et al [ 11 ] validated a method for the determination of 77 multiclass pesticides and their metabolites in Capsicum and tomato by gas and liquid chromatography tandem mass spectrometry. The method that involved extraction and purification by a modified QuEChERS approach provided high accuracy, precision, reproducibility and ruggedness, detecting and quantifying pesticide residues below their prescribed EU and FSSAI MRLs.…”
Section: Resultsmentioning
confidence: 99%
“…A Shimadzu QP2020 GC-MS (Shimadzu Corporation, Kyoto, Japan) equipped with a split-splitless-type injector was used to analyze the methanol extracts following the method described by Naik et al [18]. The mass spectrum of each original component was examined and compared to the literature data from the libraries of NIST 2017 and ADAMS-2007.…”
Section: Gc-ms Analysis Of the Methanolic Extractsmentioning
confidence: 99%
“…b The information on the analytical platform for each compound based on Almeida et al [ 136 ]. c The information on the analytical platform for each compound based on Rathod et al [ 137 ]. d The information on the analytical platform for each compound based on EPA [ 138 ].…”
Section: Applications Of Csia For Monitor Pesticide Pollution In Environments and Agricultural Productsmentioning
confidence: 99%