Abstract:An
effective and efficient method for the determination of 18 β-agonists
in aquatic products using liquid chromatography tandem mass spectrometry
(LC-MS/MS) was successfully established. The method optimization was
conducted based on incurred samples to guarantee its practicability.
In this method, the sample was hydrolyzed with β-glucuronidase-arylsulfatase
in ammonium acetate solution and treated successively with protein
precipitation in 5% trichloroacetic acid in water, lipid removal with n-hexane, and fur… Show more
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