Determination and Control of Pesticide Residues in Beverages: A Review of Extraction Techniques, Chromatography, and Rapid Detection Methods

Xu, Meng-Lei; Liu, Jingbo; Lü, Jing

doi:10.1080/05704928.2013.803978

Cited by 46 publications

(14 citation statements)

References 171 publications

Supporting

Mentioning

Contrasting

Order By: Relevance

“…If the pesticides cannot degrade naturally, they will permeate into pulp and juice and become more difficult to be removed. Thus, pesticides and their metabolites and degradation products are likely to exist in fruit juice products especially when mechanical procedures are used for extraction during postprocessing . Carbamate pesticides including insecticides, herbicides, and fungicides are a large group of synthetic pesticides replacing organochlorine and organophosphorus pesticides due to their broad biological activity, less sustainability, and relatively low mammalian toxicity .…”

Section: Introductionmentioning

confidence: 99%

Graphene‐based pipette tip solid‐phase extraction with ultra‐high performance liquid chromatography and tandem mass spectrometry for the analysis of carbamate pesticide residues in fruit juice

Shi

et al. 2016

J of Separation Science

View full text Add to dashboard Cite

Graphene-based pipette tip solid-phase extraction was combined with ultra-high performance liquid chromatography and tandem mass spectrometry for the determination of carbamate pesticide residues in fruit juice samples. Four milligrams of graphene was used as sorbent material to pack a 1000 μL pipette tip for the extraction of pirimicarb, propoxur, isoprocarb, fenobucarb, and diethofencarb from 3 mL of fruit juice sample. The whole extraction process was finished in 12 min, and the volume of eluent used was only 1.5 mL. Under the optimized conditions, good linear relationship (R > 0.999) and lower limits of detection (0.0022-0.033 ng/mL) were achieved. The recoveries at three spiked levels ranged from 80.90 to 124.60% with relative standard deviations less than 4.88%. Compared with commercially available sorbents including propylsulfonic acid silica, graphitized carbon black, and C , graphene was superior in extraction efficiency. The proposed method is simple, rapid, sensitive, selective, and solvent saving.

show abstract

Section: Introductionmentioning

confidence: 99%

Graphene‐based pipette tip solid‐phase extraction with ultra‐high performance liquid chromatography and tandem mass spectrometry for the analysis of carbamate pesticide residues in fruit juice

Shi

et al. 2016

J of Separation Science

View full text Add to dashboard Cite

show abstract

“…Associated with health of human-beings, food safety becomes a hot research topic and, in more serious cases, causes social unrest 29 30 31 32 . Great efforts from both research institutions and government departments have been made on developing various effective techniques to secure food safety 3 33 34 35 36 37 38 . Related to farm products, food-safety accidents are often induced by pesticide residues and illegal usage of veterinary drugs 31 39 40 .…”

Section: Resultsmentioning

confidence: 99%

Mesoporous-silica nanofluidic channels for quick enrichment/extraction of trace pesticide molecules

Chen

2015

Sci Rep

View full text Add to dashboard Cite

As nanofluidic channels, uniaxially oriented mesoporous-silica is, for the first time, in-situ self-assembled in a microfluidic chip for quick enrichment/extraction of ng L−1(ppt)-level organo-phosphorous (OP) pesticide residue from aqueous solution to ethanol. This micro/nano combined pre-treatment chip is essential for following gas chromatography-mass spectrometry (GC-MS) quantitative analysis. Featuring huge surface area and dense silanol groups at the inwall surface, the mesoporous-silica is uniaxially self-assembled in a micro-reservoir to form a pile of nanofluidic channels (diameter = 2.1 nm). The captured/enriched pesticide molecules in the nanochannels can be efficiently extracted by much smaller volume of ethanol due to its much higher solubility to OP. In our affirming experiment, three mixed OP pesticides of dichlorvos, paraoxon and chlorpyrifos (in water) are captured/enriched by the nano-channels and eluted/extracted by only 0.6 mL ethanol. The whole process only takes 16 min. The GC-MS quantitative results for the extracted three pesticides indicate that the extraction recovery achieves 80%. The achieved limit of quantification (LOQ) and the limit of detection (LOD) are 100 ng L−1 and 30 ng L−1, respectively. The nanofluidic-channel pre-treatment technique is promising in various application fields like agriculture and food safety security.

show abstract

“…Such a dynamic system requires adequate technologies for the detection of chemical (e.g., pesticides or drug resides) and biological contaminants (bacteria, viruses and parasites). Analytical methods used for detecting chemical agents in food are gas and liquid chromatography, often in combination with mass spectrometry [ 7 ]. Biological detection, on the other hand, can be performed using traditional microbiological culturing, electrophoresis and polymerase chain reaction-based methods.…”

Section: Introductionmentioning

confidence: 99%

Imprinted Polymers as Synthetic Receptors in Sensors for Food Safety

et al. 2021

View full text Add to dashboard Cite

Foodborne illnesses represent high costs worldwide in terms of medical care and productivity. To ensure safety along the food chain, technologies that help to monitor and improve food preservation have emerged in a multidisciplinary context. These technologies focus on the detection and/or removal of either biological (e.g., bacteria, virus, etc.) or chemical (e.g., drugs and pesticides) safety hazards. Imprinted polymers are synthetic receptors able of recognizing both chemical and biological contaminants. While numerous reviews have focused on the use of these robust materials in extraction and separation applications, little bibliography summarizes the research that has been performed on their coupling to sensing platforms for food safety. The aim of this work is therefore to fill this gap and highlight the multidisciplinary aspects involved in the application of imprinting technology in the whole value chain ranging from IP preparation to integrated sensor systems for the specific recognition and quantification of chemical and microbiological contaminants in food samples.

show abstract

Determination and Control of Pesticide Residues in Beverages: A Review of Extraction Techniques, Chromatography, and Rapid Detection Methods

Cited by 46 publications

References 171 publications

Graphene‐based pipette tip solid‐phase extraction with ultra‐high performance liquid chromatography and tandem mass spectrometry for the analysis of carbamate pesticide residues in fruit juice

Graphene‐based pipette tip solid‐phase extraction with ultra‐high performance liquid chromatography and tandem mass spectrometry for the analysis of carbamate pesticide residues in fruit juice

Mesoporous-silica nanofluidic channels for quick enrichment/extraction of trace pesticide molecules

Imprinted Polymers as Synthetic Receptors in Sensors for Food Safety

Contact Info

Product

Resources

About