Design, performance and analysis of thermal lag of the UFS1 twin-calorimeter chip for fast scanning calorimetry using the Mettler-Toledo Flash DSC 1

Herwaarden, Sander van; Iervolino, E.; Herwaarden, Floor van; Wijffels, Ties; Leenaers, A.C.H.I.; Mathot, Vincent

doi:10.1016/j.tca.2011.05.025

Cited by 188 publications

(113 citation statements)

References 7 publications

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“…But for the small sample shown in Fig. 1 the thermal lag should be a concern when rates above 10,000 K s À1 are used [26,33], which is not the case of experiment described in this work. The reason for the dramatic broadening of the relaxation peak is not known yet.…”

Section: Discussionmentioning

confidence: 86%

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Enthalpy relaxation of selenium observed by fast scanning calorimetry

et al. 2015

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Section: Discussionmentioning

confidence: 86%

“…Fast scanning calorimeter (FSC) [24,25] uses a twin-chip sensor designed for the Mettler Toledo Flash 1 DSC [26,27]. The construction of the calorimeter is described in [24,28,29].…”

Section: Methodsmentioning

confidence: 99%

Enthalpy relaxation of selenium observed by fast scanning calorimetry

et al. 2015

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“…A Mettler Flash DSC 1 was employed [32][33][34]. This is a chip based fast scanning device with power compensation.…”

Section: Fast Scanning Calorimetrymentioning

confidence: 99%

Experimental study of crystallization of PolyEtherEtherKetone (PEEK) over a large temperature range using a nano-calorimeter

et al. 2014

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“…30°C at q ? = 1000°C s -1 ), it is relatively high compared to what could be predicted based on the studies performed at optimum thermal transfer conditions for indium [33] and polyethylene films [34]. However, it has to be noted that the experimental conditions were significantly different in case of the currently discussed study [13].…”

Section: Profile Of the Thermal Gradientmentioning

confidence: 62%

Glass transition kinetics measured by fast scanning calorimetry

Svoboda

2015

J Therm Anal Calorim

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Enthalpy relaxation data obtained for amorphous selenium by means of fast scanning calorimetry were described in terms of Tool-Narayanaswamy-Moynihan model. The effect of thermal gradients formed within the measured sample was found to explain the marked difference between the FSC and conventional DSC data obtained for a-Se. If the influence of thermal gradients is accounted for, the similar set of TNM parameters as obtained for a-Se from conventional DSC can be used to describe the FSC data. Temperature profiles of the thermal gradients as well as sources of additional uncertainties occurring within the introduced conception are discussed in detail. In addition, a normalization procedure accounting for the difference between the slopes of heat capacity in the glass and undercooled liquid regions was introduced. Correct data preparation was found to have a critical influence on the applied enthalpy relaxation evaluation procedures. Due to the unresolved issue of the prediction of manifesting thermal gradients found in case of the recent study on amorphous selenium, the FSC technique appears, for the time being, to have limited usage for enthalpy relaxation studies.

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Design, performance and analysis of thermal lag of the UFS1 twin-calorimeter chip for fast scanning calorimetry using the Mettler-Toledo Flash DSC 1

Cited by 188 publications

References 7 publications

Enthalpy relaxation of selenium observed by fast scanning calorimetry

Enthalpy relaxation of selenium observed by fast scanning calorimetry

Experimental study of crystallization of PolyEtherEtherKetone (PEEK) over a large temperature range using a nano-calorimeter

Glass transition kinetics measured by fast scanning calorimetry

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