Design Consideration of Continuous-Flow Photoreactors

Protti, Stefano; Ravelli, Davide; Fagnoni, Maurizio

doi:10.1142/9781786342195_0001

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Photoredox Catalysis For the Synthesis Of Fine Chemicals And...1

Reaction Chemistry and Engineering Review1

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2023

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Cited by 7 publications

(2 citation statements)

References 56 publications

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“…• The material of the photomicroreactor is also important for high energetic efficiency, as it must have a high light transmission and low scattering in the intended wavelength. 51…”

Section: Photoredox Catalysis For the Synthesis Of Fine Chemicals And...mentioning

confidence: 99%

“…• The material of the photomicroreactor is also important for high energetic efficiency, as it must have a high light transmission and low scattering in the intended wavelength. 51 • If the device aims to carry out photochemical reactions, the microreactor must be radiation transparent. 52 Glass, quartz, silicon, and polymers are the most often utilized materials for this end.…”

Section: Reaction Chemistry and Engineering Reviewmentioning

confidence: 99%

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Combining computational fluid dynamics, photon fate simulation and machine learning to optimize continuous-flow photocatalytic systems

et al. 2023

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“…• The material of the photomicroreactor is also important for high energetic efficiency, as it must have a high light transmission and low scattering in the intended wavelength. 51…”

Section: Photoredox Catalysis For the Synthesis Of Fine Chemicals And...mentioning

confidence: 99%

Section: Reaction Chemistry and Engineering Reviewmentioning

confidence: 99%

Combining computational fluid dynamics, photon fate simulation and machine learning to optimize continuous-flow photocatalytic systems

et al. 2023

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Continuous Flow for the Photochemical C‐H Amination of Arenes

et al. 2018

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The direct C−H amination of arenes by aminium radicals generated by photolysis of N‐chloroamines is demonstrated under continuous flow conditions. The reactions proceed with comparable efficiency to small scale batch processes but are superior to larger scale batch operations. The continuous generation of the N‐chloroamine from the amine precursor can be integrated into the process, facilitating the continuous direct conversion of secondary amines to their arylated derivatives.

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Multi‐Step Continuous Flow Synthesis of β/γ‐Substituted Ketones

et al. 2018

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The smooth preparation of β/γ‐substituted ketones has been carried out by using a three‐step continuous flow synthesis involving the initial photocatalyzed addition of an aldehyde onto phenyl vinyl sulfone. The resulting β‐ketosulfones were then elaborated in flow to prepare in situ an enone upon basic elimination of the sulfonyl group and then to give γ‐nitroketones, a 4‐chromanone, and β‐(3‐indolyl)ketones in moderate to good yields.

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Design Consideration of Continuous-Flow Photoreactors

Cited by 7 publications

References 56 publications

Combining computational fluid dynamics, photon fate simulation and machine learning to optimize continuous-flow photocatalytic systems

Combining computational fluid dynamics, photon fate simulation and machine learning to optimize continuous-flow photocatalytic systems

Continuous Flow for the Photochemical C‐H Amination of Arenes

Multi‐Step Continuous Flow Synthesis of β/γ‐Substituted Ketones

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