“…Introduction: Bismuth oxybromide (BiOBr) as an important semiconductor material prefers to crystallise in tetragonal structure, a layered one to be accumulated by [Bi 2 O 2 ] 2+ slabs [1]. This structural feature together with a suitable band gap (2.75 eV) enables it a possible candidate for photocatalysis in the visible-light region [2][3][4]. Up to now various BiOBr micro/ nanostructures, including nanosheets [5][6][7][8], mesoporous structures [9,10], 3D hierarchical spheres [11][12][13][14][15][16][17], and four-leaf clover shape [18], have been successfully fabricated by means of one-step chemical synthesis, such as hydrothermal [6,7,11,13,18], solvothermal [9,10,12,16,17], ionic liquid-assisted [5,15], and microwave-assisted methods [9,14].…”