“…Yield: 78.2 mg, starting from 62.5 mg of 1 a (81%) ( 9, 142.7, 136.8, 125.3, 125.13, 125.08, 122.0, 73.8, 73.1, 29.9; GC-MS (EI, 70 eV): m/z = 318 (M + , 55), 303 (100), 300 (42), 171 (11), 147 (18), 129 (23), 115 (14), 89 (31); HRMS-ESI (m/z): [(MÀ H 2 O + H) + ] cald for (C 11 H 10 IS) + : 300.9542; found: 300.9556. 13 C NMR (CDCl 3 , 125 MHz): δ = 151. 5, 142.7, 137.1, 125.4, 125.0, 124.9, 122.0, 75.8, 73.4, 34.2, 28.3, 8.0; GC-MS (EI, 70 eV): m/z = 332 (M + , 26), 303 (100), 161 (12), 147 (12), 89 ( 14 1- 9, 141.4, 140.8, 138.0, 128.6, 128.3, 126.6, 125.5, 125.3, 125.2, 122.6, 79.3, 74.6 [b] 17 68…”