2017
DOI: 10.1590/1981-6723.6217
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Decomposição de amostras de cerveja com sistema de refluxo para determinação monoelementar por F AAS/AES e determinação multielementar por MIP OES

Abstract: Resumo Neste trabalho, é descrito o desenvolvimento de um método analítico para análise de amostras de cervejas por técnicas de espectrometria. As amostras foram preparadas por decomposição em meio ácido, em um sistema de refluxo, e as determinações foram realizadas por F AAS (Fe, Mg e Zn), F AES (Na) e MIP OES (Ca, Fe, K, Mg, Mn, Na, Ni e Zn). As melhores condições para a decomposição da amostra foram obtidas através de estudo com delineamento composto central rotacional: volume de 10,0 mL de cerveja desgasei… Show more

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Cited by 4 publications
(5 citation statements)
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“…These values are lower than those obtained by Tozetto et al (2019), who found levels of zinc (0.04 mg/L), iron (0.06 mg/L) and copper (0.23 mg/L) in craft beer produced using ginger. In general, the mineral contents in soursop fruit beer were lower than those reported in the literature and it is believed that this is related to lower turbidity and the quantities of raw material (hops and malt) in its formulation (De Leão et al, 2018).…”
Section: Centesimal and Mineral Compositionmentioning
confidence: 55%
“…These values are lower than those obtained by Tozetto et al (2019), who found levels of zinc (0.04 mg/L), iron (0.06 mg/L) and copper (0.23 mg/L) in craft beer produced using ginger. In general, the mineral contents in soursop fruit beer were lower than those reported in the literature and it is believed that this is related to lower turbidity and the quantities of raw material (hops and malt) in its formulation (De Leão et al, 2018).…”
Section: Centesimal and Mineral Compositionmentioning
confidence: 55%
“…In the mineral contents (Supplementary Table A ), the potassium and the magnesium were higher 1661.17 ppm, 486.50 ppm in black wheat beer than control white wheat beer 526.13 ppm, 126.80 ppm respectively. In addition, the calcium and zinc were also higher in black wheat beer 20.97 ppm, 1.62 ppm than the white wheat beer 8.33 ppm, 0.22 respectively 48 .…”
Section: Resultsmentioning
confidence: 83%
“…These results are shown in Table 4. Since MIP OES is a multielemental technique (Diniz et al, 2017;Leão et al, 2018;Ozbek & Akman, 2016a, 2016bOzbek et al, 2016;Williams et al, 2017) and the results obtained for Fe in the samples were statistically comparable with those obtained by F AAS, this technique was considered adequate to determine not only Fe but also other metallic elements, which concentrations should be easier detectable by MIP OES than by F AAS.…”
Section: Mineral Determinationsmentioning
confidence: 72%
“…On the other hand, higher plasma temperatures compared to flame and graphite furnace allows carbide formation or refractive element determination. Therefore, MIP OES is a cheap, practical, fast, and environmental friendly technique recently employed for multi-element determination in different food matrices, including vinegars (Ozbek et al, 2016), cheese and other dairy products (Diniz et al, 2017;Ozbek & Akman, 2016b;Williams et al, 2017), in addition to bread (Ozbek & Akman, 2016a) and beer (Leão et al, 2018).…”
Section: Introductionmentioning
confidence: 99%