During seismic slip, the elastic strain energy released by the wall rocks drives grain fragmentation and flash heating in the slipping zone, resulting in formation of (nano)powders and melt droplets, which lower the fault resistance. With progressive seismic slip, the frictional melt covers the slip surface and behaves as a lubricant reducing the coseismic fault strength. However, the processes associated to the transition from grain fragmentation to bulk frictional melting remain poorly understood. Here we discuss in situ microanalytical investigations performed on experimentally produced solidified frictional melts from the transition regime between grain fragmentation and frictional melting. The experiments were performed on granitic gneiss at seismic slip rates (1.3 and 5 m/s), normal stresses ranging from 3 to 30 MPa. At normal stresses <12 MPa, the apparent friction coefficient μ app (shear stress versus normal stress) evolves in a complex manner with slip: μ app decreases because of flash weakening, increases up to a peak value μ p1~0 .6-1.0, slightly decreases and increases again to a second peak value μ p2~0 .44-0.83, and eventually decreases with displacement to a steady-state value μ ss~0 .3-0.45. In situ synchrotron observations of the solidified frictional melt show abundance of ultrafine quartz grains before μ p2 and enrichment in SiO 2 at μ p2 . Because partial melting occurs on the ultrafine quartz grains and, as a consequence, it suggested that the second re-strengthening (μ p2 ) is induced by the higher viscosity of the melt due to its enrichment in Si from melting of the ultrafine quartz grains derived from grain fragmentation.
Key Points:• Granitic rocks sheared at seismic slip velocities and low normal stress show double-strengthening friction evolution before final weakening • Particle size distribution constrained by in situ synchrotron analysis shows the presence of additive ultrafine quartz grains • The re-strengthening was due to viscous frictional melts by quasi-equilibrium melting and the Gibbs-Thomson effect on quartz grains