“…4 is the DSC plots for samples S6, S7 and S8 taken at a heating rate of 20 K/min. It is noted that no distinguished glass transition was identified on these curves, which is in agreement with the previous results [8,9] that the samples were also prepared by chemical reduction. All these curves have a single exothermic peak, which further confirms that these three samples were indeed amorphous, and suggests that their crystallization occurred in a single-stage process corresponding to the simultaneous precipitation of crystalline phases.…”