Crystal structure of poly[aqua(μ₂-2,5-bis(4-pyridyl)-1,3,4-oxadiazole-κ² N,N)(μ₂-1,3-phenylenediacetato-κ³ O,O′:O′′)cobalt(II)], C₂₂H₁₈CoN₄O₆

Abstract

CCDC no.: 1469999Tables 1-3 contain details of the measurement method and a list of the atoms including atomic coordinates and displacement parameters. Source of materialO-phenylenediacetic acid (H 2 phda) (19 mg, 0.1 mmol), 2,5-bis(4-pyridyl)-1,3,4-oxadiazole (bpo) (22 mg, 0.1 mmol), Co(OAc) 2 ·4H 2 O (24 mg, 0.1 mmol) and KOH (5.6 mg, 0.1 mmol) were added to water (12 mL) in a Te on-lined stainless steel vessel. The mixture was heated at 433 K for 3 d, and then slowly cooled down to room temperature. Pink block crystals of the title complex were obtained.