Crystal structure of m-dichlorobis(1,10-phenanthroline)rhodium(III) Perchlorate, C24H16Cl3N4O4Rh

Ji, Zhiqin; Shan, Yongkui; Guadalupe, Ana R.; Huang, Songping D.

doi:10.1515/ncrs-1999-0345

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¹H, ¹³C and ¹⁵N NMR coordination shifts in gold(III), cobalt(III), rhodium(III) chloride complexes with pyridine, 2,2′‐bipyridine and 1,10‐phenanthroline

Pazderski

Toušek

Sitkowski

et al. 2006

Magnetic Reson in Chemistry

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Au(III), Co(III) and Rh(III) chloride complexes with pyridine (py), 2,2'-bipyridine (bpy) and 1,10-phenanthroline (phen) of the general formulae [M1LCl3], trans-[M2L4Cl2]+, mer-[M2L3Cl3], [M1(LL)Cl2]+, cis-[M2(LL)2Cl2]+, where M1=Au; M2=Co, Rh; L=py; LL=bpy, phen, were studied by 1H--13C HMBC and 1H--15N HMQC/HSQC. The 1H, 13C and 15N coordination shifts (the latter from ca-78 to ca-107 ppm) are discussed in relation to the type of metal, electron configuration, coordination sphere geometry and the type of ligand. The 13C and 15N chemical shifts were also calculated by quantum-chemical NMR methods, which reproduced well the experimental tendencies concerning the coordination sphere geometry and the ligand type.

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¹H, ¹³C and ¹⁵N NMR coordination shifts in gold(III), cobalt(III), rhodium(III) chloride complexes with pyridine, 2,2′‐bipyridine and 1,10‐phenanthroline

Pazderski

Toušek

Sitkowski

et al. 2006

Magnetic Reson in Chemistry

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show abstract

15N and 31P NMR Coordination Shifts in Transition Metal Complexes with Nitrogen- and Phosphorus-Containing Heterocycles

Pazderski

2013

Annual Reports on NMR Spectroscopy

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The crystal and molecular structure of potassium aquapentachloroiridate(III) and the 1H, 13C, 15N NMR coordination shifts in iridium(III) chloride complexes with 2,2′-bipyridine or 1,10-phenanthroline

Pazderski¹,

Toušek²,

Wojtczak³

et al. 2008

Polyhedron

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Crystal structure of m-dichlorobis(1,10-phenanthroline)rhodium(III) Perchlorate, C24H16Cl3N4O4Rh

Abstract: = 0.063, T= 296 K.

Cited by 4 publications

References 1 publication

¹H, ¹³C and ¹⁵N NMR coordination shifts in gold(III), cobalt(III), rhodium(III) chloride complexes with pyridine, 2,2′‐bipyridine and 1,10‐phenanthroline

¹H, ¹³C and ¹⁵N NMR coordination shifts in gold(III), cobalt(III), rhodium(III) chloride complexes with pyridine, 2,2′‐bipyridine and 1,10‐phenanthroline

15N and 31P NMR Coordination Shifts in Transition Metal Complexes with Nitrogen- and Phosphorus-Containing Heterocycles

The crystal and molecular structure of potassium aquapentachloroiridate(III) and the 1H, 13C, 15N NMR coordination shifts in iridium(III) chloride complexes with 2,2′-bipyridine or 1,10-phenanthroline

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Crystal structure of m-dichlorobis(1,10-phenanthroline)rhodium(III) Perchlorate, C24H16Cl3N4O4Rh

Abstract: = 0.063, T= 296 K.

Cited by 4 publications

References 1 publication

1H, 13C and 15N NMR coordination shifts in gold(III), cobalt(III), rhodium(III) chloride complexes with pyridine, 2,2′‐bipyridine and 1,10‐phenanthroline

1H, 13C and 15N NMR coordination shifts in gold(III), cobalt(III), rhodium(III) chloride complexes with pyridine, 2,2′‐bipyridine and 1,10‐phenanthroline

15N and 31P NMR Coordination Shifts in Transition Metal Complexes with Nitrogen- and Phosphorus-Containing Heterocycles

The crystal and molecular structure of potassium aquapentachloroiridate(III) and the 1H, 13C, 15N NMR coordination shifts in iridium(III) chloride complexes with 2,2′-bipyridine or 1,10-phenanthroline

Contact Info

Product

Resources

About

¹H, ¹³C and ¹⁵N NMR coordination shifts in gold(III), cobalt(III), rhodium(III) chloride complexes with pyridine, 2,2′‐bipyridine and 1,10‐phenanthroline

¹H, ¹³C and ¹⁵N NMR coordination shifts in gold(III), cobalt(III), rhodium(III) chloride complexes with pyridine, 2,2′‐bipyridine and 1,10‐phenanthroline