2017
DOI: 10.1515/ncrs-2016-0310
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Crystal structure of trans-bis((E)-7-oxo-4-(phenyldiazenyl)cyclohepta-1,3,5-trien-1-olato)-κ2 O,O′)-bis(pyridine-κN)cobalt(II), C36H28CoN6O4

Abstract: The crystal structure is shown in the figure. Tables 1 and 2 contain details on crystal structure and measurement conditions and a list of the atoms including atomic coordinates and displacement parameters. Source of materialThe reagents available commercially were used without further purification. 5-(Phenyldiazenyl)tropolone was synthesized according to the previously published method [3]. 5-(Phenyldiazenyl)tropolone (452 mg, 2.0 mmol) and pyridine (162 µL, 2.0 mmol) were added to a solution of Co(CH 3 COO)… Show more

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