Crystal structure of tert-butyl 2-phenylethylcarbamate, C₁₃H₁₉NO₂

Abstract

CCDC no.: 1487250The asymmetric unit of the title structure is shown in the gure. Tables 1 and 2 contain details of the measurement method and a list of the atoms including atomic coordinates and displacement parameters. Source of materialtert-Butyl 2-phenylethylcarbamate was synthesized from the reaction of 2-phenylethylamine with 1.2 equivalents of ditert-butyl dicarbonate in the presence of 1.5 equivalents of triethylamine in dichloromethane at 0°C for 15 minutes and

MethylN-(2-bromo-4-chlorophenyl)carbamate

“…They can be synthesized using a variety of convenient processes (Blaser et al, 2012;Smith et al, 2012;Ibrahim et al, 2011;Porzelle et al, 2009;Lee et al, 2009;Lebel & Leogane, 2006;Caddick et al, 2003). The X-ray crystal structure of the related tert-butyl 2-phenylethylcarbamate was published recently (El-Hiti et al, 2016).…”