Abstract:Source of materialThe title compound was prepared following the reported procedure [1]. In a typical experiment 0.2 g (yield 89%) of the title compound was obtained. The single crystals were obtained by slow evaporation from an ethanol solution at room temperature.
Experimental detailsHydrogen atoms bonded to carbon were positioned geometrically, with C-H = 0.95 to 0.99 Å, and constrained to ride on their parent atoms, with U iso (H) =1.2U eq (C). Positional parameters and the U iso value of the hydrogen atom … Show more
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