Abstract:C 11 H 12 Cl 2 N 4 OZn, triclinic, P1 (no. 2), a =7.487(2) Å, b =8.604(2) Å, c =11.952(2) Å, a =69.13(3)°, b =80.47(3)°,
Source of materialAs olution of the 3-[3-(pyridin-2-yl)-1H-pyrazol-1-yl]propanamide ligand (0.0432 g, 0.2 mmol) in acetonitrile (15 ml) was added dropwise to asolution of ZnCl 2 (0.0272 g, 0.2 mmol) in methanol (10 ml) in a50mlbeaker. The mixture was stirred for 30 min at 323 K, then filtered. The resulted solution was kept at room temperature. Colorless block-shaped single crystals suitable… Show more
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