Crystal structure of bis(benzene-1 carboxylato-O 3,5-carboxyl-κ ¹O)-[(5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ ⁴ N,N′,N′′,N′′′)nickel(II) ─ benzene-1,3,5-tricarboxylic acid ─ water (1/2/4), C₅₂H₆₆N₄NiO₂₈

Abstract

C52H66N4NiO28, triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 11.292(6) Å, b = 11.670(6) Å, c = 12.165(6) Å, α = 81.872(6)°, β = 67.036(5)°, γ = 75.624(6)°, V = 1428.1(12) Å3, Z = 1, Rgt (F) = 0.0439, wRref (F 2) = 0.1216, T = 296(2) K.