Crystal structure of bis(2,4-dibromo-6-{(E)[(4-fluorobenzyl)imino]methyl}phenolato-κ² N,O) copper(II), C₂₈H₁₈Br₄F₂N₂O₂Cu

Abstract

C 28 H 18 Br4CuF 2 N 2 O 2 , monoclinic, C2 (no. 5), a = 14.6518(8) Å, CCDC no.: 1449858The crystal structure is shown in the gure. Tables 1-3 contain details of the measurement method and a list of the atoms including atomic coordinates and displacement parameters. Source of material3,5-dibromo-2-hydroxybenzaldehyde 2.80 g (10 mmol) and (4-uorobenzyl)methanamine 1.25 g (10 mmol) were dissolved in ethanol and stirred for 2 h at a temperature of 65°C. After evaporation, a crude product was recrystallized twice