C11H 12 N 2 O 3 , monoclinic, P21/n (no. 14), a = 8.1726(2) Å, b = 7.1419(2) Å, c = 18.4875(6) Å, β = 100.376(1), V = 1061.43(4) Å 3 ,
CCDC no.: 1536055The crystal structure is shown in the figure. Tables 1 and 2 contain details on crystal structure and measurement conditions and a list of the atoms including atomic coordinates and displacement parameters.
Source of materialPyrrolidine (5.46 g, 66 mmol) and sodium hydrogenocarbonate (5.54 g, 66 mmol) were added to 2-chloro-5-