Abstract:Source of materialIn at ypical synthesis, 3-carboxyl-1-(4-carboxylphenylmethylene)-2-oxidopyrinium (0.029g ,0 .13 mmol), CuCl 2 ×2H 2 O (0.021 g, 0.13 mmol), and pyrazino[2,3-f]-[1,10]phenanthroline (0.034, 0.13 mmol) were dissolved in the mixure of DMF (6 ml) and water (2 ml) under stirring. This mixture was sealed into a 15 ml autoclave and heated in the oven up to 358 Kfor 4days. After cooling to room temperature, the blue block-shaped crystals were collectedasasinglephase.
Experimental detailsThecarbonH-at… Show more
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